Green Synthesis of Trimetallic Ni–Co–Mo incorporated into Biomass-Derived Porous Carbon for Advanced Supercapacitor Applications | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Green Synthesis of Trimetallic Ni–Co–Mo incorporated into Biomass-Derived Porous Carbon for Advanced Supercapacitor Applications Aruna Thaker, Tajala Magray, Arwa makki, Dina Hajjar, Balasaheb Nagare, and 1 more This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-8956091/v1 This work is licensed under a CC BY 4.0 License Status: Posted Version 1 posted You are reading this latest preprint version Abstract This study reports two-step synthesis strategy employing bio-mass derived carbon obtained from cutch tree (Acacia catechu) bark which is subsequently incorporated into the nickel, cobalt, and molybdenum (NCMO) trimetallic oxide systems. A homogeneous dispersion of trimetallic oxides within the carbon matrix (NCM/AC), leads to notable alterations in both the surface morphology and crystalline characteristics of the synthesized nanocomposite. This Structural regulation effectively mitigates phase segregation and the enhanced accessibility of electrochemically active sites through structural regulation sites, thereby delivering a specific capacitance of 503 F g -1 at a current density of 1 A g -1 . Furthermore, the Hybrid supercapacitor device (HSD) based on the NCM/AC composite exhibits, retaining its electrochemical performance over 10,000 charge-discharge cycles at current density 5 A g -1 . Overall, our work demonstrates an environmentally benign and sustainable synthesis route that combines ternary metal oxides with biomass-derived activated carbon to produce efficient electrode materials suitable for advanced energy storage systems. Transition metal Bio-mass supercapacitor carbon and trimetallic Full Text Additional Declarations No competing interests reported. Cite Share Download PDF Status: Posted Version 1 posted You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. Our growing team is made up of researchers and industry professionals working together to solve the most critical problems facing scientific publishing. Also discoverable on Platform About Our Team In Review Editorial Policies Advisory Board Help Center Resources Author Services Accessibility API Access RSS feed Manage Cookie Preferences © Research Square 2026 | ISSN 2693-5015 (online) Privacy Policy Terms of Service Do Not Sell My Personal Information {"props":{"pageProps":{"initialData":{"identity":"rs-8956091","acceptedTermsAndConditions":true,"allowDirectSubmit":true,"archivedVersions":[],"articleType":"Research Article","associatedPublications":[],"authors":[{"id":616545559,"identity":"b3c86d0f-6182-4cd1-8788-97c43229caa4","order_by":0,"name":"Aruna Thaker","email":"","orcid":"","institution":"University of Mumbai","correspondingAuthor":false,"prefix":"","firstName":"Aruna","middleName":"","lastName":"Thaker","suffix":""},{"id":616545560,"identity":"b48d903b-0b1d-43dc-8941-500b07e11be6","order_by":1,"name":"Tajala Magray","email":"","orcid":"","institution":"University of Mumbai","correspondingAuthor":false,"prefix":"","firstName":"Tajala","middleName":"","lastName":"Magray","suffix":""},{"id":616545561,"identity":"7ea2c232-0e2b-4f29-a314-e1680f05c513","order_by":2,"name":"Arwa makki","email":"","orcid":"","institution":"Jeddah University","correspondingAuthor":false,"prefix":"","firstName":"Arwa","middleName":"","lastName":"makki","suffix":""},{"id":616545562,"identity":"118d0aff-5604-43aa-8d86-f4746be8e5da","order_by":3,"name":"Dina Hajjar","email":"","orcid":"","institution":"Jeddah University","correspondingAuthor":false,"prefix":"","firstName":"Dina","middleName":"","lastName":"Hajjar","suffix":""},{"id":616545563,"identity":"d56ce04d-96fc-4f6d-aa99-1983fb8ff5da","order_by":4,"name":"Balasaheb Nagare","email":"","orcid":"","institution":"University of Mumbai","correspondingAuthor":false,"prefix":"","firstName":"Balasaheb","middleName":"","lastName":"Nagare","suffix":""},{"id":616545564,"identity":"2246b3c5-2fbf-41eb-a9df-698605aa8ef0","order_by":5,"name":"Pradip Sarawade","email":"data:image/png;base64,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","orcid":"","institution":"University of Mumbai","correspondingAuthor":true,"prefix":"","firstName":"Pradip","middleName":"","lastName":"Sarawade","suffix":""}],"badges":[],"createdAt":"2026-02-24 10:24:42","currentVersionCode":1,"declarations":"","doi":"10.21203/rs.3.rs-8956091/v1","doiUrl":"https://doi.org/10.21203/rs.3.rs-8956091/v1","draftVersion":[],"editorialEvents":[],"editorialNote":"","failedWorkflow":false,"files":[{"id":107234882,"identity":"f1186373-9d8d-4268-80c0-33778cdd9192","added_by":"auto","created_at":"2026-04-19 01:54:18","extension":"pdf","order_by":1,"title":"","display":"","copyAsset":false,"role":"manuscript-pdf","size":1109330,"visible":true,"origin":"","legend":"","description":"","filename":"Manuscript.pdf","url":"https://assets-eu.researchsquare.com/files/rs-8956091/v1_covered_b306a07f-348e-43a9-b5c9-2b106aef107b.pdf"}],"financialInterests":"No competing interests reported.","formattedTitle":"Green Synthesis of Trimetallic Ni–Co–Mo incorporated into Biomass-Derived Porous Carbon for Advanced Supercapacitor Applications","fulltext":[],"fulltextSource":"","fullText":"","funders":[],"hasAdminPriorityOnWorkflow":false,"hasManuscriptDocX":false,"hasOptedInToPreprint":true,"hasPassedJournalQc":"","hasAnyPriority":false,"hideJournal":true,"highlight":"","institution":"","isAcceptedByJournal":false,"isAuthorSuppliedPdf":true,"isDeskRejected":"","isHiddenFromSearch":false,"isInQc":false,"isInWorkflow":false,"isPdf":true,"isPdfUpToDate":true,"isWithdrawnOrRetracted":false,"journal":{"display":true,"email":"
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