Developing of tunable attenuatter of laser beam via ZnSe thin films

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Abstract Zinc selenide thin films (ZnSe) were prepared using (ZnCl2 & Na2SeO3) compounds by deposited by spray pyrolysis technique on glass substrates under the temperature of( 200 C°), with different molar concentrations (0.05-0.075-0.1) mol/L and then annealed at a temperature of (450 C°), where it is observed that when the molar concentration increases, the thickness increases and also when the temperature increases, The results of (FE-SEM) that the surface composition has changed from a spherical Particles shape of thin films before annealing to regular, more compact spherical shapes within the Nanoscale range and smaller size. As for the results of the optical properties, it noted that the value of absorbance increases with increasing molar concentration at the point of absorption in the wavelength (320nm) before and after annealing, the results of the Photoluminescence (PL) examination Approached the visible when the violet color before annealing, after annealing, it approached more to the ultraviolet area, as well as the intensity increased, but when the concentration increased, we get the excitement of higher intensity and it was found that the band gap increases with increasing concentration (3.52- 3.70)eV and also increases after annealing (3.60 – 3.76)eV. The Laser (PSU-H-FDA) with a wavelength (473nm) and pulse laser device of the type (Fiber Laser-1064nm-100W), the input power (130 mW),(34W) respectively for all thin films it was found that the highest attenuation of laser radiation was at the higher concentration(0.1mol/L) the lower the Power transmittance(25mW) and (11W) as well as after annealing.
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Developing of tunable attenuatter of laser beam via ZnSe thin films | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Developing of tunable attenuatter of laser beam via ZnSe thin films Suroor Mahdi, Huda Saadi Ali This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-4462884/v1 This work is licensed under a CC BY 4.0 License Status: Under Review Version 1 posted 3 You are reading this latest preprint version Abstract Zinc selenide thin films (ZnSe) were prepared using (ZnCl2 & Na2SeO3) compounds by deposited by spray pyrolysis technique on glass substrates under the temperature of( 200 C°), with different molar concentrations (0.05-0.075-0.1) mol/L and then annealed at a temperature of (450 C°), where it is observed that when the molar concentration increases, the thickness increases and also when the temperature increases, The results of (FE-SEM) that the surface composition has changed from a spherical Particles shape of thin films before annealing to regular, more compact spherical shapes within the Nanoscale range and smaller size. As for the results of the optical properties, it noted that the value of absorbance increases with increasing molar concentration at the point of absorption in the wavelength (320nm) before and after annealing, the results of the Photoluminescence (PL) examination Approached the visible when the violet color before annealing, after annealing, it approached more to the ultraviolet area, as well as the intensity increased, but when the concentration increased, we get the excitement of higher intensity and it was found that the band gap increases with increasing concentration (3.52- 3.70)eV and also increases after annealing (3.60 – 3.76)eV. The Laser (PSU-H-FDA) with a wavelength (473nm) and pulse laser device of the type (Fiber Laser-1064nm-100W), the input power (130 mW),(34W) respectively for all thin films it was found that the highest attenuation of laser radiation was at the higher concentration(0.1mol/L) the lower the Power transmittance(25mW) and (11W) as well as after annealing. Thin film Optical mirror Annealing Reflection Full Text Additional Declarations No competing interests reported. Cite Share Download PDF Status: Under Review Version 1 posted Editor assigned by journal 04 Jun, 2024 Submission checks completed at journal 23 May, 2024 First submitted to journal 22 May, 2024 You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. Our growing team is made up of researchers and industry professionals working together to solve the most critical problems facing scientific publishing. Also discoverable on Platform About Our Team In Review Editorial Policies Advisory Board Help Center Resources Author Services Accessibility API Access RSS feed Manage Cookie Preferences © Research Square 2026 | ISSN 2693-5015 (online) Privacy Policy Terms of Service Do Not Sell My Personal Information {"props":{"pageProps":{"initialData":{"identity":"rs-4462884","acceptedTermsAndConditions":true,"allowDirectSubmit":false,"archivedVersions":[],"articleType":"Research Article","associatedPublications":[],"authors":[{"id":310334687,"identity":"eb0249fa-607c-4a4d-8edd-6a8c9c3b1bb3","order_by":0,"name":"Suroor Mahdi","email":"data:image/png;base64,iVBORw0KGgoAAAANSUhEUgAAAZAAAAAyAQMAAABI0h/eAAAABlBMVEX///8AAABVwtN+AAAACXBIWXMAAA7EAAAOxAGVKw4bAAAA70lEQVRIiWNgGAWjYBADGTb25uMfPgBZbOxEauFh4zmWxjgDpIWZWC0MEjlmzDwgJiEt8jNyHz74uMeOhw+o5bHNr23yfMwMjB8+5uDWYnAj3dhwxrNkoMOelRvn9t02bGNmYJacuQ2PFok0NmmeA8w8bOzJG6Rze24zArWwMfPi0SI/A6ylnoeNIcFA2rLntj1BLQw3wFoO87BxpJhJM/y4nUhQi8GZZ8yGMw4cBwVysmFvw+3kNmbGZrx+kW9PY3zw4UC1nHx788EHP/7ctp0PZHz4iM9hKICxDUw2EKseBP6QongUjIJRMApGCgAALJdJwNnN7iYAAAAASUVORK5CYII=","orcid":"","institution":"Tikrit University","correspondingAuthor":true,"prefix":"","firstName":"Suroor","middleName":"","lastName":"Mahdi","suffix":""},{"id":310334688,"identity":"3c2dcdb7-5799-4538-a21b-a5cf3ce07201","order_by":1,"name":"Huda Saadi Ali","email":"","orcid":"","institution":"Al-Karkh University of Science","correspondingAuthor":false,"prefix":"","firstName":"Huda","middleName":"Saadi","lastName":"Ali","suffix":""}],"badges":[],"createdAt":"2024-05-22 19:53:24","currentVersionCode":1,"declarations":"","doi":"10.21203/rs.3.rs-4462884/v1","doiUrl":"https://doi.org/10.21203/rs.3.rs-4462884/v1","draftVersion":[],"editorialEvents":[],"editorialNote":"","failedWorkflow":false,"files":[{"id":57761458,"identity":"73b51831-c944-4133-aa98-3fcedc236875","added_by":"auto","created_at":"2024-06-05 09:37:45","extension":"pdf","order_by":1,"title":"","display":"","copyAsset":false,"role":"manuscript-pdf","size":908641,"visible":true,"origin":"","legend":"","description":"","filename":"DevelopingoftunableattenuatteroflaserbeamviaZnSethinfilms.pdf","url":"https://assets-eu.researchsquare.com/files/rs-4462884/v1_covered_5db464e8-35fb-4f0d-9d42-91a371c5ad7f.pdf"}],"financialInterests":"No competing interests reported.","formattedTitle":"Developing of tunable attenuatter of laser beam via ZnSe thin films","fulltext":[],"fulltextSource":"","fullText":"","funders":[],"hasAdminPriorityOnWorkflow":false,"hasManuscriptDocX":false,"hasOptedInToPreprint":true,"hasPassedJournalQc":"","hasAnyPriority":false,"hideJournal":false,"highlight":"","institution":"","isAcceptedByJournal":false,"isAuthorSuppliedPdf":true,"isDeskRejected":"","isHiddenFromSearch":false,"isInQc":false,"isInWorkflow":false,"isPdf":true,"isPdfUpToDate":true,"isWithdrawnOrRetracted":false,"journal":{"display":true,"email":"[email protected]","identity":"applied-physics-b","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":false,"externalIdentity":"aphb","sideBox":"Learn more about [Applied Physics B](http://link.springer.com/journal/340)","snPcode":"340","submissionUrl":"https://submission.nature.com/new-submission/340/3","title":"Applied Physics B","twitterHandle":"","acdcEnabled":true,"dfaEnabled":true,"editorialSystem":"em","reportingPortfolio":"Springer Hybrid","inReviewEnabled":true,"inReviewRevisionsEnabled":false},"keywords":"Thin film, Optical mirror, Annealing, Reflection","lastPublishedDoi":"10.21203/rs.3.rs-4462884/v1","lastPublishedDoiUrl":"https://doi.org/10.21203/rs.3.rs-4462884/v1","license":{"name":"CC BY 4.0","url":"https://creativecommons.org/licenses/by/4.0/"},"manuscriptAbstract":"\u003cp\u003eZinc selenide thin films (ZnSe) were prepared using (ZnCl2 \u0026amp; Na2SeO3) compounds by deposited by spray pyrolysis technique on glass substrates under the temperature of( 200 C°), with different molar concentrations (0.05-0.075-0.1) mol/L and then annealed at a temperature of (450 C°), where it is observed that when the molar concentration increases, the thickness increases and also when the temperature increases, The results of (FE-SEM) that the surface composition has changed from a spherical Particles shape of thin films before annealing to regular, more compact spherical shapes within the Nanoscale range and smaller size. 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