Experimental setup for the determination of spectral normal emissivity of conductive materials in the wavelength range of 1-18 µm and the temperature range of 300 - 1700 o C in the air

Experimental setup for the determination of spectral normal emissivity of conductive materials in the wavelength range of 1-18 µm and the temperature range of 300 - 1700 o C in the air | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Experimental setup for the determination of spectral normal emissivity of conductive materials in the wavelength range of 1-18 µm and the temperature range of 300 - 1700 o C in the air R. A. Mironov, A. E. Kryukov, A. O. Zabezhaylov, M. O. Zabezhaylov, and 1 more This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-4766080/v1 This work is licensed under a CC BY 4.0 License Status: Published Journal Publication published 08 Oct, 2024 Read the published version in Applied Physics B → Version 1 posted 8 You are reading this latest preprint version Abstract This article describes the measurement procedure and data processing features of an apparatus for measuring the spectral emissivity of electrically conductive opaque materials in the air. The developed laboratory setup has the following three main features: induction heating of the sample, correction in order to exclude the surrounding radiation reflected by the sample, and the use of multiwavelength pyrometry. Single-sided induction heating of the sample eliminates the contribution of stray radiation from the heating element to the recorded signal. The correction on surrounding radiation increases the accuracy of emissivity determination, especially at low temperatures. The multiwavelength pyrometry is used to obtain the true temperature of a sample. This technique makes it possible to obtain the surface temperature of the sample directly from its thermal radiation spectrum, allowing to examine the material during the oxidation process. The emissivity spectra of zirconium and hafnium diboride samples were measured with the created setup. The obtained spectra reveal several features, which correlate with chemical transformations on the surface of the materials during oxidation. Full Text Additional Declarations No competing interests reported. Cite Share Download PDF Status: Published Journal Publication published 08 Oct, 2024 Read the published version in Applied Physics B → Version 1 posted Editorial decision: Revision requested 16 Sep, 2024 Reviews received at journal 30 Aug, 2024 Reviewers agreed at journal 09 Aug, 2024 Reviewers agreed at journal 01 Aug, 2024 Reviewers invited by journal 01 Aug, 2024 Editor assigned by journal 27 Jul, 2024 Submission checks completed at journal 19 Jul, 2024 First submitted to journal 19 Jul, 2024 You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. Our growing team is made up of researchers and industry professionals working together to solve the most critical problems facing scientific publishing. Also discoverable on Platform About Our Team In Review Editorial Policies Advisory Board Help Center Resources Author Services Accessibility API Access RSS feed Manage Cookie Preferences © Research Square 2026 | ISSN 2693-5015 (online) Privacy Policy Terms of Service Do Not Sell My Personal Information {"props":{"pageProps":{"initialData":{"identity":"rs-4766080","acceptedTermsAndConditions":true,"allowDirectSubmit":false,"archivedVersions":[],"articleType":"Research Article","associatedPublications":[],"authors":[{"id":338914915,"identity":"df568d06-9286-4b90-9901-7abc499c0a2c","order_by":0,"name":"R. A. Mironov","email":"data:image/png;base64,iVBORw0KGgoAAAANSUhEUgAAAZAAAAAyAQMAAABI0h/eAAAABlBMVEX///8AAABVwtN+AAAACXBIWXMAAA7EAAAOxAGVKw4bAAAAuUlEQVRIiWNgGAWjYBADORAhQZIWY9K1JDYQrUW3/ezBzxUV29I3HD978MbHNoZ8gwMEtJidyUuWPHPmdu4GIMNyxhkGyw0EtRzIMZBsbANqOZBjJs1TwWBA2Jbzb4x/ArWkG5x/Yyb9x4AYLTdyzEC2JBgAGdIMRNly442ZZcOZ24Yzb7wxtuw5I2EgSdhhOcY3Gypuy/OdzzG88bPNxoCPkBY4UICoJCU25RtIUDwKRsEoGAUjCwAAIoJGBOLX130AAAAASUVORK5CYII=","orcid":"","institution":"ORPE “Technologiya” named after A.G. Romashin","correspondingAuthor":true,"prefix":"","firstName":"R.","middleName":"A.","lastName":"Mironov","suffix":""},{"id":338914916,"identity":"0f2a2c27-7da2-423b-9c01-2cd2bed1ed14","order_by":1,"name":"A. E. Kryukov","email":"","orcid":"","institution":"ORPE “Technologiya” named after A.G. Romashin","correspondingAuthor":false,"prefix":"","firstName":"A.","middleName":"E.","lastName":"Kryukov","suffix":""},{"id":338914917,"identity":"7b5d6f22-345b-40e9-8713-eb54c1c67ac8","order_by":2,"name":"A. O. Zabezhaylov","email":"","orcid":"","institution":"ORPE “Technologiya” named after A.G. Romashin","correspondingAuthor":false,"prefix":"","firstName":"A.","middleName":"O.","lastName":"Zabezhaylov","suffix":""},{"id":338914918,"identity":"d48a75d9-3704-43c0-b437-cc5155e9c9f8","order_by":3,"name":"M. O. Zabezhaylov","email":"","orcid":"","institution":"ORPE “Technologiya” named after A.G. Romashin","correspondingAuthor":false,"prefix":"","firstName":"M.","middleName":"O.","lastName":"Zabezhaylov","suffix":""},{"id":338914919,"identity":"f84617a7-058a-4a72-8ddd-c730b3995e79","order_by":4,"name":"M. Y. Rusin","email":"","orcid":"","institution":"ORPE “Technologiya” named after A.G. Romashin","correspondingAuthor":false,"prefix":"","firstName":"M.","middleName":"Y.","lastName":"Rusin","suffix":""}],"badges":[],"createdAt":"2024-07-19 04:12:51","currentVersionCode":1,"declarations":"","doi":"10.21203/rs.3.rs-4766080/v1","doiUrl":"https://doi.org/10.21203/rs.3.rs-4766080/v1","draftVersion":[],"editorialEvents":[{"content":"https://doi.org/10.1007/s00340-024-08331-9","type":"published","date":"2024-10-08T15:57:16+00:00"}],"editorialNote":"","failedWorkflow":false,"files":[{"id":66597329,"identity":"c0f35550-79ec-4c09-8580-115cdc82e9a8","added_by":"auto","created_at":"2024-10-14 16:09:37","extension":"pdf","order_by":1,"title":"","display":"","copyAsset":false,"role":"manuscript-pdf","size":1797151,"visible":true,"origin":"","legend":"","description":"","filename":"Mironov24forIJThermophysics.pdf","url":"https://assets-eu.researchsquare.com/files/rs-4766080/v1_covered_1d4b13c6-8bfc-45b5-97dc-26be96afdb83.pdf"}],"financialInterests":"No competing interests reported.","formattedTitle":"Experimental setup for the determination of spectral normal emissivity of conductive materials in the wavelength range of 1-18 µm and the temperature range of 300 - 1700 o C in the air","fulltext":[],"fulltextSource":"","fullText":"","funders":[],"hasAdminPriorityOnWorkflow":false,"hasManuscriptDocX":false,"hasOptedInToPreprint":true,"hasPassedJournalQc":"","hasAnyPriority":false,"hideJournal":false,"highlight":"","institution":"","isAcceptedByJournal":true,"isAuthorSuppliedPdf":true,"isDeskRejected":"","isHiddenFromSearch":false,"isInQc":false,"isInWorkflow":false,"isPdf":true,"isPdfUpToDate":true,"isWithdrawnOrRetracted":false,"journal":{"display":true,"email":"[email protected]","identity":"applied-physics-b","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":false,"externalIdentity":"aphb","sideBox":"Learn more about [Applied Physics B](http://link.springer.com/journal/340)","snPcode":"340","submissionUrl":"https://submission.nature.com/new-submission/340/3","title":"Applied Physics B","twitterHandle":"","acdcEnabled":true,"dfaEnabled":true,"editorialSystem":"em","reportingPortfolio":"Springer Hybrid","inReviewEnabled":true,"inReviewRevisionsEnabled":false},"keywords":"","lastPublishedDoi":"10.21203/rs.3.rs-4766080/v1","lastPublishedDoiUrl":"https://doi.org/10.21203/rs.3.rs-4766080/v1","license":{"name":"CC BY 4.0","url":"https://creativecommons.org/licenses/by/4.0/"},"manuscriptAbstract":"This article describes the measurement procedure and data processing features of an apparatus for measuring the spectral emissivity of electrically conductive opaque materials in the air. The developed laboratory setup has the following three main features: induction heating of the sample, correction in order to exclude the surrounding radiation reflected by the sample, and the use of multiwavelength pyrometry. Single-sided induction heating of the sample eliminates the contribution of stray radiation from the heating element to the recorded signal. The correction on surrounding radiation increases the accuracy of emissivity determination, especially at low temperatures. The multiwavelength pyrometry is used to obtain the true temperature of a sample. This technique makes it possible to obtain the surface temperature of the sample directly from its thermal radiation spectrum, allowing to examine the material during the oxidation process. The emissivity spectra of zirconium and hafnium diboride samples were measured with the created setup. The obtained spectra reveal several features, which correlate with chemical transformations on the surface of the materials during oxidation.","manuscriptTitle":"Experimental setup for the determination of spectral normal emissivity of conductive materials in the wavelength range of 1-18 µm and the temperature range of 300 - 1700 o C in the air","msid":"","msnumber":"","nonDraftVersions":[{"code":1,"date":"2024-08-14 19:18:25","doi":"10.21203/rs.3.rs-4766080/v1","editorialEvents":[{"type":"communityComments","content":0},{"type":"decision","content":"Revision requested","date":"2024-09-16T12:50:59+00:00","index":"","fulltext":""},{"type":"editorInvitedReview","content":"","date":"2024-08-30T16:57:30+00:00","index":"hide","fulltext":""},{"type":"reviewerAgreed","content":"183310382807853197138882748225472929116","date":"2024-08-09T09:28:37+00:00","index":"hide","fulltext":""},{"type":"reviewerAgreed","content":"164429060921914244250620725195409561309","date":"2024-08-01T16:43:24+00:00","index":"hide","fulltext":""},{"type":"reviewersInvited","content":"","date":"2024-08-01T10:04:04+00:00","index":"","fulltext":""},{"type":"editorAssigned","content":"","date":"2024-07-27T06:59:34+00:00","index":"","fulltext":""},{"type":"checksComplete","content":"","date":"2024-07-19T15:13:09+00:00","index":"","fulltext":""},{"type":"submitted","content":"Applied Physics B","date":"2024-07-19T04:11:24+00:00","index":"","fulltext":""}],"status":"published","journal":{"display":true,"email":"[email protected]","identity":"applied-physics-b","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":false,"externalIdentity":"aphb","sideBox":"Learn more about [Applied Physics B](http://link.springer.com/journal/340)","snPcode":"340","submissionUrl":"https://submission.nature.com/new-submission/340/3","title":"Applied Physics B","twitterHandle":"","acdcEnabled":true,"dfaEnabled":true,"editorialSystem":"em","reportingPortfolio":"Springer Hybrid","inReviewEnabled":true,"inReviewRevisionsEnabled":false}}],"origin":"","ownerIdentity":"5e8eb8b7-1db5-465d-b54e-b5bd2306c7bb","owner":[],"postedDate":"August 14th, 2024","published":true,"recentEditorialEvents":[],"rejectedJournal":[],"revision":"","amendment":"","status":"published-in-journal","subjectAreas":[],"tags":[],"updatedAt":"2024-10-14T16:04:37+00:00","versionOfRecord":{"articleIdentity":"rs-4766080","link":"https://doi.org/10.1007/s00340-024-08331-9","journal":{"identity":"applied-physics-b","isVorOnly":false,"title":"Applied Physics B"},"publishedOn":"2024-10-08 15:57:16","publishedOnDateReadable":"October 8th, 2024"},"versionCreatedAt":"2024-08-14 19:18:25","video":"","vorDoi":"10.1007/s00340-024-08331-9","vorDoiUrl":"https://doi.org/10.1007/s00340-024-08331-9","workflowStages":[]},"version":"v1","identity":"rs-4766080","journalConfig":"researchsquare"},"__N_SSP":true},"page":"/article/[identity]/[[...version]]","query":{"redirect":"/article/rs-4766080","identity":"rs-4766080","version":["v1"]},"buildId":"qtupq5eGEP_6zYnWcrvyt","isFallback":false,"isExperimentalCompile":false,"dynamicIds":[84888],"gssp":true,"scriptLoader":[]}