Total Synthesis of Putative Xestocyclamine A

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AI-generated summary by claude@2026-07, 2026-07-15

This study reports the first total synthesis of putative xestocyclamine A, an important intermediate in polycyclic alkaloid biosynthesis, but the synthetic compound's spectral data deviate from previously reported data.

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Abstract

The first total synthesis of putative xestocyclamine A (-)- 1 is reported, a compound taking center stage on the the pathway explaining the biosynthesis of a prominent family of polycyclic alkaloids (Baldwin-Whitehead pathway). The identity of the synthetic sample is unambiguous but the recorded spectral data deviate from those of xestocyclamine A reported in the literature.

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europepmc
last seen: 2026-05-19T01:45:01.086888+00:00