Comparison of Volatile Compounds of Some Medicinal Plants from Lamiaceae Family by HS-SPME Method

Comparison of Volatile Compounds of Some Medicinal Plants from Lamiaceae Family by HS-SPME Method | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Comparison of Volatile Compounds of Some Medicinal Plants from Lamiaceae Family by HS-SPME Method Zeynep Ergun, Elmira Ziya Motalebipour, Mujgan Guney, Esra Gölcü, and 1 more This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-8966477/v1 This work is licensed under a CC BY 4.0 License Status: Posted Version 1 posted You are reading this latest preprint version Abstract This study investigates the volatile compounds in twelve medicinal plants from the Lamiaceae family using headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry (HS-SPME/GC-MS). Lamiaceae plants are recognized for their diverse medicinal properties, including antioxidative, antibacterial, and antifungal effects. A total of 74 volatile compounds were identified, encompassing terpenes, alcohols, esters, aldehydes, and ketones. Notably, Lavandula spica L. exhibited the highest number of unique volatiles (28), while Melissa officinalis L. had the fewest (16). Key compounds included Citral (65.48%) in Melissa officinalis L., Menthol (33.37%) and Menthyl acetate (30.53%) in Mentha piperita L., Carvone (45.86%) in Mentha spicata L., and Eucalyptol (54.71%) in Origanum syriacum L. Plants from Adana Botanic Park were rich in terpenes and ketones, whereas those from Osmaniye contained higher levels of alcohols, aldehydes, and esters. The findings emphasize the impact of geographic location on volatile profiles and suggest avenues for further research into medicinal efficacy and optimal dosage. Lamiaceae Medicinal Plant Volatile compounds HS-SPME GC–MS Figures Figure 1 Figure 2 Figure 3 Introduction The Lamiaceae family, comprising 236 genera and 6900 to 7200 species, stands out as one of the most significant herbal families due to its diverse array of medicinal plants [ 1 ]. Among the prominent genera with notable medicinal potential are Lavandula , Mentha , Melissa , Origanum , Rosmarinus , Salvia , Sideritis , and Thymus [ 2 ]. Lavenders ( Lavandula spp.), a standout member of the Lamiaceae family, include more than 39 species distributed across Arabia, the Mediterranean region, Asia, Northern Africa, and the Middle East [ 3 ]. Lavandula species are characterized by aromatic compounds such as linalool, α-pinene, limonene, cineole, cis- and trans-ocimene, 3-octanone, camphor, caryophyllene, and terpinene-4-ol (Hajhashemi et al. 2004). Lavandula spica L. and Lavandula dentata L., which are endemic and widely distributed in the Mediterranean part of Turkey, hold special importance. Lavender is in high demand in flavoring, food, and pharmaceutical industries due to its robust aroma [ 4 ] A study indicated that the use of lavender oil aromatherapy among individuals diagnosed with fibromyalgia led to a significant enhancement in their quality of life [ 5 ]. The Mentha genus, comprising 18 species, is another famous source of medicinal herbs within the Lamiaceae family. This genus is widely distributed in North America, Europe, Asia, and Africa. Mints are valued for their anti-inflammatory and analgesic properties, making them a valuable tool in folk medicine for addressing various ailments. Among the main species within this genus are Mentha spicata and Mentha piperita L. Mentha piperita L. is a hybrid of M. spicata and M. aquatic . The key components extracted from Mentha are identified as menthol, Menthone, and 1,8 cineol [ 6 ]. The Melissa genus stands out as an aromatic herb within the Lamiaceae family, with its native range encompassing Europe, Asia, southwestern Siberia, and northern Africa. Notably, Melissa Officinalis L., known as lemon balm, English balm, and sweet balm, is another member of the mint family. Key compounds present in M. Officinalis L. include citronellol, citral, and linalool [ 7 ]. These compounds contribute to its antiviral and antibacterial effects, making it a valuable treatment for ailments caused by viruses and bacteria. Origanum genus is a subshrub within the Lamiaceae family, native to Europe, Asia, and North Africa. This genus is pivotal in traditional medicine, particularly in addressing respiratory complaints. With over 18 hybrids and 43 species, Origanum holds significant diversity [ 8 ]. Origanum Majorana L., Origanum syriacum var. bevanii , and Origanum syriacum L. are endemic species, widely distributed in the Mediterranean region. Notable compounds found in the Origanum genus include terpinene-4-ol, cis-sabinene, and o-cymene, with their quantities varying among different species [ 9 ]. Rosmarinus officinalis L., commonly known as rosemary, is a perennial herbaceous plant renowned for its antioxidant and anti-inflammatory properties which also belongs to the Lamiaceae family and is native to the Mediterranean region. However, due to its valuable culinary and medicinal attributes, it has been widely cultivated across the globe [ 3 ]. The versatility of Rosmarinus officinalis L. (rosemary) is evident through its extensive use in the realms of cooking, medicine, and cosmetics. Its robust flavor and aromatic qualities have contributed to its popularity as a culinary ingredient, while its therapeutic potential has been acknowledged for centuries [ 3 ]. Beyond its culinary and medicinal roles, rosemary's antibacterial and antifungal attributes have led to its inclusion in aromatherapy, where it is believed to aid in stress reduction and memory enhancement. The compound makeup of rosemary is notably rich in terpenes, including alpha-pinene, beta-pinene, and camphor. These constituents contribute to its distinct properties and applications [ 10 ]. Salvia L., commonly referred to as sage, is a notable genus within the mint family, Lamiaceae. This genus encompasses a diverse array of plants, exceeding 900 species that are distributed globally, primarily in temperate regions. Among the prominent members of the Salvia genus, Salvia Officinalis L. holds particular significance. This species boasts a broad spectrum of primary and secondary metabolites, contributing to its valuable medicinal and nutritional attributes. Secondary metabolites in Salvia Officialis L. include terpenoids, phenolic acids, flavonoids, and tannins. Notably, terpenoids such as thujone, camphor, and cineole are present, each possessing distinct medicinal properties. Thujone, for instance, has been linked to various effects, while camphor and cineole are recognized for their antimicrobial and antifungal properties. These compounds collectively contribute to the diverse therapeutic potential associated with sage [ 11 ]. Sideritis spp., commonly referred to as mountain tea, stands as a noteworthy genus of flowering plants within the Lamiaceae family. Indigenous to the Mediterranean region, this genus has gained popularity as an herbal tea. With a substantial presence of over 150 species, Sideritis has a rich history in traditional medicine due to its recognized anti-inflammatory, antioxidant, and antimicrobial attributes. In more recent times, scientific exploration has illuminated the potential of Sideritis as a treatment for Alzheimer's disease and other neurological disorders. This research has underscored its significance beyond traditional applications [ 12 ]. The secondary metabolites found within Sideritis spp., notably rosmarinic acid and apigenin, are particularly noteworthy for their significant antioxidant and anti-inflammatory properties. These compounds contribute to the diverse therapeutic potential of Sideritis , making it a valued herbal remedy with potential implications for various health conditions [ 13 ]. Thymus L., a perennial shrub belonging to the Lamiaceae family, is more commonly recognized as thyme. Originating in the Mediterranean region, this plant has been cultivated and valued for its aromatic and medicinal attributes over many centuries. Among the various species within this genus, Thymus vulgaris L. stands out, renowned for its remarkable medicinal qualities. This species has earned a prominent place as a natural remedy, addressing an array of health concerns including respiratory infections, digestive troubles, and inflammatory conditions. The therapeutic potential of Thymus vulgaris L. can be attributed to its composition, which is rich in compounds like thymol and carvacrol. These bioactive constituents contribute to the plant's antibacterial, antiviral, and antifungal properties. The presence of these compounds underscores its traditional and contemporary uses as a powerful and versatile herbal remedy [ 14 ]. Indeed, the medicinal plant species within the Lamiaceae family hold considerable significance in natural medicine, pharmacology, cosmetology, and aromatherapy due to their diverse secondary metabolites. These include alcohols, aldehydes, ketones, esters, terpenes, and phenolic compounds, which confer antimicrobial, antiviral, antioxidant, and anti-inflammatory activities [15; 16; 17]. Despite extensive studies on essential oils of Lamiaceae species obtained mainly through hydrodistillation, little is known about their volatile composition when analyzed using solvent-free techniques that preserve thermolabile and low-volatility compounds. Moreover, the influence of distinct microclimates on the volatile profiles of these medicinal plants remains underexplored. Therefore, the novelty of this study lies in applying HS-SPME/GC-MS to comparatively profile the volatiles of 12 medicinal plants collected from two different Turkish provinces (Adana and Osmaniye), thereby addressing the gap in knowledge on how geographical origin affects volatile composition when assessed by this technique. Materials and Methods Material Twelve distinct members of the Lamiaceae plant family, including Sweet Marjoram, Lemon Balm, Bible Hyssop, Hybrid Mint, Greek Sage, Lavender, Fringed Lavender, Za'atar, Spearmint, Rosemary, Sage, and Thyme, without undergoing any treatments, were used in the current study. The plant materials were collected from Ali Nihat Gokyigit Botanical Garden (n = 7) and Osmaniye (n = 5) in July 2019 (Table 1 ). Formal taxonomic identification of the plant material was performed by Dr. Zeynep Ergun based on regional floristic references and morphological characteristics. A voucher specimen of this material was not deposited in publicly accessible herbarium. Following collection, the plant samples were appropriately labeled based on their origin and were subsequently stored at a temperature of -20°C. For subsequent analyses, one gram of each ground plant material. Table 1 Studied twelve different species of Lamiaceae family NO Name Species Place of Collection 1 Lavender Lavandula Spica L. Adana Botanik Park 2 Fringed Lavender or French Lavender, Lavandula Dentata L. Adana Botanik Park 3 Lemon Balm Melissa Officinalis L. Adana Botanik Park 4 Spearmint, Garden Mint, Common Mint, Lamb Mint, Mackerel Mint Mentha Spicata L. Osmaniye 5 Hybrid Mint (Peppermint ) Mentha Piperita L. Osmaniye 6 Marjoram Origanum Majorana L. Adana Botanik Park 7 Bible Hyssop, Biblical-Hyssop, Lebanese Oregano, Syrian Oregano Origanum syriacum var. bevanii Adana Botanik Park 8 Za'atar Origanum syriacum L. Adana Botanik Park 9 Rosemary Rosmarinus officinalis L. Osmaniye 10 Common Sage, Sage Salvia officinalis L. Osmaniye 11 Greek Sage Sideritis spp. Adana Botanik Park 12 Common Thyme, German Thyme, Garden Thyme, Thyme Thymus Vulgaris L. Osmaniye Methods HS-SPME extraction of volatile compounds Volatile compounds were extracted using the Headspace-Solid Phase Microextraction (HS-SPME) technique. Ground samples were homogenized with 5 M calcium chloride (CaCl₂) to increase ionic strength and facilitate the release of volatile compounds into the headspace, as described in similar extraction protocols [ 18 ]. A 100 µm PDMS fiber was employed because it is widely used for monoterpene-rich matrices such as Lamiaceae essential oils. Although a CAR/PDMS fiber was also tested, PDMS fiber yielded a higher number of compounds in our samples, and therefore was selected for subsequent analyses. The fiber was exposed to the sample headspace and incubated for 30 min at 30°C with magnetic stirring. The extraction time was chosen based on preliminary trials showing equilibrium after 30 min, consistent with literatures [ 18 ]. GC/MS analysis Analysis was conducted using a Shimadzu GC/MS equipped with a DB-Wax column (30 m × 0.25 mm × 0.5 µm). Helium was used as the carrier gas at a flow rate of 1.4 mL/min (adjusted to the optimal linear velocity for this column). The oven temperature program started at 40°C, increased at 10°C/min to 200°C (16 min), and was held for 10 min, giving a total run time of ~ 26 min. This correction addresses a discrepancy in the original text regarding ramp duration. Compound identification was performed tentatively by comparing mass spectra with NIST/Wiley libraries and retention indices. Retention indices were calculated against a C7–C30 n-alkane series under identical conditions, and reference RI values for DB-Wax were obtained from the NIST database. Quantification was expressed as relative percentage of total ion current (TIC) peak areas, which provides semi-quantitative comparison among samples but does not account for compound-specific ionization efficiencies. All analyses were performed in triplicate. Relative standard deviations (RSD%) were calculated for major compounds to assess analytical precision. Result and discussion Volatile Compound of Lamiaceae Family Table 2 includes information on the percentage component distribution, retention time, and retention indices for each volatile compound identified in the studied samples. Detected volatile compounds within the Lamiaceae family encompass a diverse array of chemical family groups, comprising 3 volatiles in aldehydes, 23 volatiles in alcohols, 7 volatiles in esters, 3 volatiles in ketones, and 37 volatiles in terpenes. Out of the 74 volatile compounds investigated in this study, terpenes exhibited the widest diversity, while the smallest range was observed in aldehydes (Fig. 1 ). The presence of volatile compounds varied in terms of abundance across different species, ranging from high to low quantities. Additionally, certain compounds were not detected in certain studied species. Terpenes were found to have the highest percentage of volatiles, whereas esters exhibited the lowest percentage. Among the volatile compounds, terpenes emerged as the dominant category for the Lamiaceae family species. The investigation encompassing 12 distinct Lamiaceae species yielded diverse volatile compound profiles. Specifically, Lavandula Spica L. featured 28 volatiles, while Lavandula Dentata L. and Mentha Spicata each contained 23 volatiles. Mentha Piperita L. exhibited 20 volatiles, Melissa Officinalis L. had 16, and Origanum Majorana L. had 25. Notably, Origanum syriacum var. bevanii showcased 22, while Origanum syriacum L. and Rosmarinus officinalis L. each featured 21 and 26 volatiles, respectively. Salvia officinalis L. contained 21 volatiles, Sideritis spp. L. had 18, and Thymus Vulgaris L. featured 24. The most extensive and least extensive species-specific volatile components were observed in Lavandula Spica L. with 28 volatiles and Melissa Officinalis L. with 16 volatiles, respectively (Table 2 ). Table 2 Number of Aroma Compounds per Chemical Family in 12 Species of Lamiacea Family. NO Chemical family/Species Aldehydes Alcohols Esters Ketones Terpenes 1 Lavandula Spica L. 0 8 0 2 18 2 Lavandula Dentata L. 0 7 2 2 12 3 Melissa Officinalis L. 2 6 2 0 6 4 Mentha Spicata L. 1 8 2 3 9 5 Mentha Piperita L. 1 6 1 0 12 6 Origanum Majorana L. 2 4 3 0 16 7 Origanum syriacum var. bevanii 1 8 1 1 10 8 Origanum syriacum L. 1 9 1 0 11 9 Rosmarinus officinalis L. 0 9 1 2 14 10 Salvia officinalis L. 0 5 1 1 14 11 Sideritis spp. 0 3 0 0 14 12 Thymus Vulgaris L. 0 9 2 1 12 In various species of the Lamiaceae family, the terpenes category exhibited notable high-quantity compounds such as eucalyptol, p-cymene, α-thujone, trans-sabinene hydrate, caryophyllene, and β-Pinene. Among the alcohols chemical family, l-(-)-menthol, α-terpineol, 1-Borneol, and Linalool were found in significant quantities. Notably, the esters category was characterized by high quantities of Menthyl acetate and neryl acetate. In terms of aldehydes, citral emerged as a high-quantity compound. Lastly, carvone and camphor stood out as compounds of substantial quantity within the ketones category (Table 3 ). This comprehensive study underscores the diverse range of volatile compounds within different Lamiaceae species. Significant percentages of volatile compounds were identified in specific species. For instance, citral from the Aldehyde chemical family was notably present in Melissa Officinalis L. at a percentage of 65.48%. Among the Alcohols chemical family, L(-)Menthol was detected in Mentha Piperita L. at a level of 33.37%. Menthyl acetate categorized within the Ester chemical family, stood out in Mentha Piperita L. at a level of 30.53%. Within the Ketones chemical family, carvone was identified in Mentha Spicata L. at a percentage of 45.86%. Noteworthy, eucalyptol, a member of the Terpen chemical family, was found in Origanum syriacum L. at a percentage of 54.71% (Table 3 ). Table 3 Volatile Compound, retention time, retention indices and their percentage composition of studied species of Lamiaceae family. Chemical family Compounds Name R.T RI DB*-wax 1 2 3 4 5 6 7 8 9 10 11 12 Aldehyde (E)-2-Hexenal 10.05 1228 1227 N.D. N.D. N.D. N.D. N.D. 0.8 N.D. 0.48 N.D. N.D. N.D. N.D. Citronellal 17.40 1490 1488 N.D. N.D. 0.11 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Citral 23.75 1742 1741 N.D. N.D. 65.48 2.47 0.54 8.29 1.52 N.D. N.D. N.D. 5.2 N.D. Total Aldehydes N.D. N.D. 65.59 2.47 0.54 8.29 1.52 N.D. N.D. N.D. N.D. N.D. Alcohols 1-Hexanol 13.69 1356 1359 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. (Z)-3-Hexen-1-ol 14.60 1388 1379 N.D. N.D. N.D. N.D. N.D. N.D. 0.26 N.D. N.D. N.D. N.D. N.D. 3-Octanol 14.86 1396 1393 N.D. N.D. N.D. 0.96 0.12 N.D. N.D. 1.6 N.D. N.D. N.D. N.D. 1-Octen-3-ol 16.49 1458 1450 N.D. N.D. N.D. 1.74 N.D. N.D. 0.36 1.84 N.D. 0.08 0.6 0.39 2-Ethyl-1-hexanol 17.54 1495 1495 N.D. N.D. N.D. N.D. 1.42 N.D. N.D. N.D. N.D. N.D. N.D. N.D. Linalool 19.12 1556 1556 0.79 2.21 1 0.33 5.12 13.91 0.11 0.19 3.88 0.06 N.D. 6.44 Isopulegol 19.50 1571 1571 1.46 5.53 0.12 N.D. N.D. N.D. 1.38 N.D. 0.43 N.D. N.D. N.D. Terpinen-4-ol 20.45 1607 1602 N.D. N.D. 0.06 0.23 N.D. 5.1 0.43 N.D. 0.97 N.D. N.D. N.D. L-(-)-Menthol 21.42 1647 1645 0.76 3.95 N.D. N.D. 33.37 0.36 1.92 0.19 N.D. N.D. N.D. 0.26 Pinocarveol 21.78 1661 1654 1.95 3.13 0.18 N.D. N.D. N.D. 0.36 0.54 1.08 0.38 0.21 0.33 α-Terpineol 22.80 1701 1706 1.16 1.69 N.D. N.D. N.D. 3.65 1.57 0.89 22.19 1.5 1.95 1.07 1-Borneol 22.93 1708 1706 3.7 8.4 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Lavandulol 24.30 1760 1686 0.61 0.88 N.D. N.D. N.D. N.D. N.D. N.D. 0.99 N.D. N.D. N.D. Citronellol 24.51 1774 1764 N.D. N.D. 0.6 N.D. N.D. N.D. N.D. N.D. 0.51 N.D. N.D. N.D. Nerol 25.28 1807 1797 N.D. N.D. 3.12 0.15 N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.3 trans-Carveol 26.03 1841 1833 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 1.11 N.D. N.D. N.D. Phenylethyl Alcohol 27.83 1921 1918 0.3 N.D. N.D. 0.18 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Methyleugenol 30.13 2029 2030 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Nerolidol 30.53 2049 2014 N.D. N.D. N.D. 0.14 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Carvacrol 34.03 2224 2240 N.D. N.D. N.D. 0.18 0.35 N.D. N.D. 6.09 0.56 N.D. N.D. 0.32 Veridiflorol 31.46 2093 2092 N.D. N.D. N.D. N.D. 0.12 N.D. N.D. 2.45 N.D. 1.02 N.D. 0.6 Spathulenol 35.73 2306 2129 N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.27 N.D. N.D. N.D. 0.3 Total Alcohols 10.73 25.79 5.08 1.21 38.96 23.02 5.77 10.62 31.72 0 0 0 Esters Menthyl acetate 18.69 1540 1541 N.D. N.D. N.D. 0.2 30.53 0.88 0.12 N.D. 1.34 0.54 N.D. N.D. Neryl acetate 23.64 1738 1737 N.D. 6.37 N.D. N.D. N.D. 0.17 N.D. N.D. N.D. N.D. N.D. 0.16 Geranyl acetate 24.36 1768 1768 N.D. N.D. 0.4 N.D. N.D. 0.4 N.D. N.D. N.D. N.D. N.D. N.D. p-Cumic aldehyde 24.90 1791 1794 N.D. 1.79 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Geranyl propionate 25.78 1829 1828 N.D. N.D. 0.83 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.61 Eugenol acetate 33.17 2181 2263 N.D. N.D. N.D. 0.75 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Z-3-hexenyl phenylacetate 34.32 2238 2220 N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.65 N.D. N.D. N.D. N.D. Total Esters 0 8.16 1.23 0.75 0 0.57 0 0.65 0 0 0 0 Ketones Camphor 18.20 1520 1536 15.21 29.82 N.D. 0.54 N.D. N.D. 1.49 N.D. 13.92 17.54 N.D. 0.87 Carvone 23.86 1740 1744 2.38 3.44 N.D. 45.86 N.D. N.D. N.D. N.D. 1.38 N.D. N.D. N.D. cis-Jasmone 28.13 1935 1938 N.D. N.D. N.D. 1.46 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Total Ketones 17.59 33.26 0 47.86 0 0 1.49 0 15.3 0 0 0 Terpens α-Pinene 4.98 1006 1015 3.31 N.D. 0.82 N.D. N.D. 1.36 N.D. 0.19 1.69 6.15 14.6 N.D. Camphene 5.85 1068 1059 1.3 N.D. N.D. N.D. N.D. 0.29 N.D. N.D. 1.69 7.94 N.D. N.D. β-Pinene 6.71 1102 1096 2.6 3.54 N.D. N.D. 0.5 0.7 N.D. N.D. N.D. 5.13 18.09 N.D. Sabinene 7.05 1117 1119 1.54 N.D. N.D. N.D. 0.19 9.41 N.D. N.D. N.D. 0.14 4.88 N.D. α-Phellandrene 8.23 1162 1160 N.D. N.D. N.D. N.D. N.D. 1.44 N.D. N.D. N.D. N.D. 0.96 N.D. β-Myrcene 8.34 1166 1178 N.D. N.D. 23.06 N.D. 0.54 3.33 N.D. N.D. N.D. 1.64 N.D. N.D. α-Terpinene 8.98 1188 1183 N.D. N.D. N.D. N.D. N.D. 3.06 N.D. N.D. N.D. N.D. N.D. N.D. Limonene 9.20 1195 1193 1.79 N.D. N.D. N.D. 1.34 3.38 N.D. N.D. 6.29 2.88 4.59 N.D. Eucalyptol 9.53 1207 1202 41.29 N.D. N.D. 16.27 6.31 N.D. 54.71 N.D. 22.42 11.57 N.D. N.D. γ-Terpinene 10.64 1249 1251 2.15 0.71 N.D. N.D. N.D. 5.3 1.23 2.2 N.D. 0.16 N.D. 4.6 3-Carene 10.93 1259 1162 N.D. N.D. 0.58 N.D. N.D. 0.25 N.D. N.D. N.D. N.D. 0.56 N.D. p-Cymene 11.43 1276 1275 0.45 4.83 N.D. N.D. N.D. 2.4 9.88 36.21 0.9 0.7 N.D. 27.6 α-Terpinolene 11.75 1287 1288 N.D. N.D. N.D. N.D. N.D. 1.34 N.D. N.D. N.D. 0.18 N.D. N.D. α-Fenchene 14.94 1399 1402 2.29 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. α-Thujone 15.63 1425 1416 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 30.97 N.D. 0.83 α-Cubebene 16.61 1462 1460 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 8.87 N.D. Menthone 16.78 1492 1473 N.D. N.D. N.D. N.D. 8.9 N.D. N.D. N.D. N.D. N.D. N.D. N.D. trans Sabinene hydrate 16.79 1468 1474 1.24 2.02 N.D. 1.85 N.D. 30.63 0.53 2.45 N.D. 0.59 N.D. 1.08 Menthofurane 17.46 1492 1497 N.D. N.D. N.D. N.D. 7.35 N.D. N.D. N.D. N.D. N.D. N.D. N.D. α-Copaene 17.64 1498 1491 N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.51 0.28 N.D. 9.08 0.23 β-Bourbonene 18.36 1527 1528 N.D. 1.22 N.D. 0.68 0.59 1.67 N.D. 2.2 N.D. N.D. 0.63 0.85 α-Gurjunene 18.68 1539 1529 N.D. N.D. N.D. N.D. N.D. 0.63 N.D. N.D. N.D. N.D. 3.76 N.D. (E)-Pinanone 19.00 1552 1548 N.D. N.D. N.D. N.D. 0.2 N.D. N.D. N.D. 3.56 N.D. N.D. N.D. β-Ocimene 20.14 1594 1233 0.55 1.96 N.D. N.D. N.D. N.D. 0.12 N.D. N.D. N.D. N.D. N.D. β-Elemene 20.24 1598 1599 N.D. N.D. N.D. N.D. 0.41 N.D. N.D. N.D. N.D. N.D. N.D. N.D. β-Guaiene 20.26 1599 1663 N.D. N.D. 0.06 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Caryophyllene 20.37 1603 1608 2.78 8.58 2.54 8.75 N.D. N.D. 6.72 15.88 0.7 4.62 9.82 5.65 D-Verbenone 22.98 1709 1723 0.27 1.1 N.D. N.D. N.D. N.D. N.D. N.D. 4.94 N.D. N.D. N.D. Germacrene D 23.23 1720 1710 1.94 N.D. N.D. 10.65 2.77 N.D. 0.31 4.35 0.78 N.D. 9.49 1.22 Piperitone 23.55 1734 1735 0.87 1.64 N.D. N.D. 0.7 N.D. N.D. N.D. N.D. N.D. N.D. 0.39 σ-Cadinene 24.39 1769 1749 N.D. 0.85 N.D. 0.64 N.D. N.D. N.D. 0.25 N.D. N.D. 5.08 3.07 α-Calamenene 26.12 1845 1837 N.D. 0.8 N.D. 1.66 N.D. N.D. 0.41 N.D. 2.61 N.D. N.D. 0.39 Pulegone 26.63 1867 1631 N.D. N.D. N.D. 2.75 N.D. N.D. N.D. N.D. 0.49 N.D. N.D. N.D. Thymol 33.52 2198 2146 1.41 N.D. 0.35 2.29 N.D. 1.27 14.12 20.24 0.64 4.52 1.65 42.43 Estragole 22.38 1685 1685 0.99 N.D. N.D. N.D. N.D. N.D. 2.46 0.34 4.34 N.D. N.D. N.D. Coumarin 39.95 2459 2458 3.22 4.35 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. Total Terpens 69.99 31.6 27.41 45.54 29.8 66.46 90.49 84.82 51.33 77.19 92.06 88.34 The heatmap analysis for the aroma profile of 12 species from the Lamiaceae family reveals distinct groupings of species based on their concentrations of specific chemical compounds such as alcohols, aldehydes, esters, ketones, and terpenes (Fig. 2 ). Each species exhibits a unique chemical composition that contributes to its aroma, with several notable patterns emerging from the analysis. Mentha species, including Mentha Spicata L. and Mentha Piperita L., are particularly rich in menthol, menthone, and other related compounds, placing them in a distinct cluster due to their strong minty aroma profiles. On the other hand, Melissa Officinalis L. stands out with high levels of citral, making it unique among the other species for its lemon-like scent. The presence of high aldehyde concentrations in Melissa Officinalis L. contrasts with species like Lavandula Spica L. and Lavandula Dentata L., which are rich in linalool and geranyl acetate, compounds that contribute to their sweet and floral scents commonly associated with lavender oils. The principal component analysis (PCA) also clearly separated the studied Lamiaceae species based on their volatile compound profiles obtained by HS-SPME. The first two principal components (PC1: 24.9%, PC2: 16.5%) together explained over 40% of the total variance, indicating that a considerable proportion of the chemical variation among species was captured. Samples such as Origanum syriacum and Lavandula stoechas were distinctly positioned along PC1, largely influenced by high contributions from terpenes and ketones, while Melissa officinalis and Mentha spicata clustered closer together, reflecting their higher alcohol contents. The strong loadings of compounds such as linalool, geraniol, and camphor suggest that these metabolites were the main drivers of separation among species. The PCA biplot therefore highlights the chemical diversity of Lamiaceae volatiles and demonstrates that terpenes and alcohols are the most discriminative chemical families. This chemometric approach provides a clear comparative framework, enabling differentiation of closely related taxa based on their volatile fingerprints (Fig. 3 ). Terpenes such as thymol, carvacrol, and eucalyptol are prominent in species like Thymus Vulgaris L., Origanum syriacum L., and Rosmarinus officinalis L., which group together due to their strong herbal and camphoraceous aromas, making them valuable in medicinal and antiseptic applications. The dendrogram included in the heatmap illustrates these relationships by clustering species that share similar concentrations of these key compounds. For example, the close clustering of Origanum Majorana L. and Origanum syriacum L. reflects their similar terpene profiles, while species like Sideritis spp. and Salvia officinalis L. form another cluster based on their diverse chemical makeup, particularly in terms of their high terpene content. The clustering of species based on their chemical profiles helps to identify potential uses for each plant. For instance, species high in alcohols like Linalool (e.g., lavender species) are ideal for perfumery, while those rich in menthol and menthone (e.g., mint species) are suitable for medicinal and culinary purposes. The high terpene concentrations in species like Thymus Vulgaris L. and Origanum syriacum L. highlight their antimicrobial and antifungal properties, making them valuable for therapeutic use. Overall, this heatmap analysis underscores the chemical diversity within the Lamiaceae family and provides a comprehensive framework for understanding how different species can be clustered based on their aroma profiles for various applications. Variation of volatile compounds among plant species The analysis of aromatic compounds within the Lamiaceae family has unveiled a diverse range of constituents that significantly contribute to their distinct scent profiles and potential therapeutic attributes. Within Lavandula Spica L., Eucalyptol emerges as a prominent element, constituting a significant portion (41.29%) alongside Camphor (15.21%). Eucalyptol carries a refreshing, camphor-like fragrance with a hint of peppery coolness. Its alluring aromatic and flavor qualities make it valuable in fragrances, cosmetics, and as a flavor enhancer. Eucalyptol has demonstrated antinociceptive properties, suggesting potential calming and central nervous system depressant effects [ 19 ]. Inhalation of eucalyptus aromatherapy oil, abundant in over 80% eucalyptol, has proven effective in mitigating post-COVID syndrome symptoms, such as breathlessness, back pain, and anxiety affecting individuals worldwide and potentially bearing labor and financial repercussions [ 5 ]. Furthermore, the therapeutic potential of eucalyptol spans cardiovascular treatments, antimicrobial effects, anti-inflammatory benefits, and respiratory disorder support, corroborated by numerous studies [ 1 ]. Conversely, Eucalyptol remains undetected in Lavandula Dentata L., where Camphor (29.82%), Caryophyllene (8.58%), 1-Borneol (8.4%), and Neryl acetate (6.37%) emerge as primary volatile compounds. The prevalence of camphor-rich compounds in Lavandula species is validated by multiple scientific publications [ 20 ]. However, some researchers have reported linalool as the principal compound in the essential oil of Lavandula species [ 21 ]. Both Camphor and 1-Borneol have demonstrated extensive and diverse pharmacological effects, encompassing anti-inflammatory, analgesic, and antipyretic properties and notable antimicrobial activity [ 22 ]. Melissa Officinalis L. exhibited a notable abundance of Citral (65.48%) and β-Myrcene (23.06%). Previous studies have documented the presence of Citral in Melissa species [ 23 ], while the occurrence of β-Myrcene was initially observed in this study. Myrcene finds application in cosmetics, soaps, detergents, and as a versatile food additive. It also holds a foundational role in creating essential fragrances such as menthol, citral, citronellol, and others, which are pivotal in the production of commercially significant compounds. Several studies have also revealed the properties of β-Myrcene, encompassing anxiolytic, antioxidant, anti-aging, anti-inflammatory, and analgesic attributes [ 24 ]. The dominant volatile compounds in Mentha Spicata L. were Carvone (45.86%) and eucalyptol (16.27%). On the other hand, the primary volatile compounds in Mentha Piperita L. consisted of L-(-)-Menthol (33.37%), Menthyl acetate (30.53%), Menthone (8.9%) and Eucalyptol (6.31%). The investigation by Park et al. [ 25 ] reported eucalyptol (46.28 ± 4.25), caryophyllene (5.47 ± 0.49), and menthol (3.02 ± 0.22) as the major components in Mentha spp , which are quite similar to the volatile compounds identified in the present study, although caryophyllene was found at a higher level in our results. In the current study, the highlighted volatile compounds of three Origanum species; Origanum Majorana L., Origanum syriacum L., and Origanum syriacum var. bevanii comprised trans sabinene hydrate (30.63%), eucalyptol (54.71%), p-cymene (36.21%), respectively. Terpenes have consistently emerged as the key active components in Oregano species [ 26 ]. Rosmarinus officinalis L. exhibited α-Terpineol (22.19%), camphor (13.92%), and eucalyptol (22.42%) as its primary compounds. This study marks the first time identification of α-Terpineol and eucalyptol in this context. Salvia officinalis L. featured α-thujone (30.97%) and camphor (17.54%), as its prominent volatile compounds. In the case of Sideritis spp., the major component was β-pinene (18.09%), differing from the observations of Kardali et al. [ 27 ] which α-pinene was the primary compound. Thymus Vulgaris L. demonstrated richness in thymol (42.43%) and p-cymene (27.6%). The species of Lamiaceae family for this study were collected from two distinct locations, Adana Botanik Park and Osmaniye, providing insight into the contrasting climate of these regions. The discernible differences in weather patterns and climatic attributes reflect the distinctive conditions between Osmaniye and Adana. Osmaniye in southern Turkey exhibits a Mediterranean climate characterized by hot, dry summers and moderate, wet winters. Meanwhile, Adana, located nearby, shares a Mediterranean climate but tends to be slightly warmer and more arid due to its lower elevation and proximity to the Mediterranean Sea. This results in Adana often having warmer summertime temperatures and receiving less precipitation compared to Osmaniye. Despite the overall similarity in climate, these subtle variations in temperature and rainfall underscore the existence of microclimatic nuances, even within close proximity. These factors contribute significantly to the substantial differences observed in the compounds in the current study. According to the literature review, variations in volatile compounds are influenced by factors such as location, seasonal changes, and developmental stages [28; 29]. Conclusion The Lamiaceae family includes numerous species widely used in traditional medicine. In this study, twelve species collected from Adana and Osmaniye (Turkey) exhibited diverse volatile profiles comprising aldehydes, alcohols, esters, ketones, and terpenes. Among these, terpenes were the dominant chemical group across all species, consistent with previous essential oil studies. Unlike many earlier works that applied hydrodistillation, our study utilized HS-SPME/GC-MS, which allowed detection of thermolabile and low-volatility compounds that are often lost during conventional extraction. This represents one of the first comparative HS-SPME-based surveys of multiple Lamiaceae species grown under different microclimatic conditions. The comparative results demonstrated that plants collected from Osmaniye were relatively richer in aldehydes, alcohols, and esters, whereas plants from Adana contained higher levels of ketones and terpenes. These findings highlight the significant influence of local microclimatic factors on volatile composition, an aspect rarely considered in previous research. It is important to note that the compounds were tentatively identified based on library matching and retention indices, and quantification was semi-quantitative. Therefore, results should be interpreted as relative rather than absolute concentrations. Future work should validate major compounds using pure standards, apply mixed-phase SPME fibers for broader coverage, and integrate chemometric tools (PCA, cluster analysis) to better resolve interspecies differences. Overall, this study contributes new insights into the volatile diversity of Lamiaceae species under different Turkish microclimates and demonstrates the utility of HS-SPME/GC-MS as a complementary approach to hydrodistillation. These results may support future standardization of medicinal plant products and guide cultivation strategies aimed at optimizing the yield of bioactive volatile constituents. Abbreviations All abbreviations used in this manuscript are defined and presented in the table below: HS-SPME : Headspace Solid-Phase Microextraction GC-MS : Gas Chromatography-Mass Spectrometry M. spicata : Mentha spicata M. piperita L. : Mentha piperita L. M. Officinalis L .: Melissa officinalis L. Sideritis spp .: Sideritis species TIC : Total Ion Current RSD% : Relative Standard Deviation (percentage) PDMS : Polydimethylsiloxane CAR : Carboxen NIST : National Institute of Standards and Technology RI : Retention Index PCA : Principal Component Analysis PC : Principal Component Spp .: Species Declarations Ethics Approval and Consent to Participate This study was conducted in full compliance with ethical principles, ensuring the protection of participants' rights and welfare throughout the research process. The study adhered to established ethical guidelines, and informed and voluntary consent was obtained from all participants prior to their involvement in the study. Consent for Publication This manuscript includes identifiable information of the authors (such as names and affiliations), but it does not include any identifiable information of participants (such as images, faces, or other personal data). Therefore, the "Consent for Publication" section is "NOT APPLICABLE" for this manuscript. Availability of Data and Materials All data and materials utilized in this research are available upon request. For access to the dataset or research materials, please contact the corresponding author. Competing Interests The authors declare that they have no financial or non-financial competing interests related to this research. There is no conflict of interest in the conduct or reporting of this study. Funding This research was not funded by any external organizations. The authors self-financed the study and the associated research activities. Authors' Contributions Each author has contributed significantly to the conception, design, data analysis, writing, and revision of the manuscript. The corresponding author, (name of corresponding author), supervised the submission process and coordinated revisions. 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10:23:40","currentVersionCode":1,"declarations":"","doi":"10.21203/rs.3.rs-8966477/v1","doiUrl":"https://doi.org/10.21203/rs.3.rs-8966477/v1","draftVersion":[],"editorialEvents":[],"editorialNote":"","failedWorkflow":false,"files":[{"id":104252365,"identity":"4598bc8f-f04b-49d2-9105-987379195eb7","added_by":"auto","created_at":"2026-03-09 16:18:12","extension":"png","order_by":1,"title":"Figure 1","display":"","copyAsset":false,"role":"figure","size":46155,"visible":true,"origin":"","legend":"\u003cp\u003eTotal aroma compounds (%) by chemical family in 12 species of Lamiacea family\u003c/p\u003e","description":"","filename":"1.png","url":"https://assets-eu.researchsquare.com/files/rs-8966477/v1/e2c48792d9f939938a992685.png"},{"id":104252298,"identity":"e6eb581a-e26e-4a29-8a43-5ab96c76f6d6","added_by":"auto","created_at":"2026-03-09 16:18:02","extension":"png","order_by":2,"title":"Figure 2","display":"","copyAsset":false,"role":"figure","size":327773,"visible":true,"origin":"","legend":"\u003cp\u003eHeatmap of volatile aroma profiles in 12 Lamiaceae species obtained by HS-SPME, illustrating the distribution and relative abundance of major chemical compounds across taxa.\u003c/p\u003e","description":"","filename":"2.png","url":"https://assets-eu.researchsquare.com/files/rs-8966477/v1/6ed6770a3fd3b0fe3ea7d199.png"},{"id":104252367,"identity":"07ef0b56-efb5-4b42-bbe2-bc471f0a6568","added_by":"auto","created_at":"2026-03-09 16:18:12","extension":"png","order_by":3,"title":"Figure 3","display":"","copyAsset":false,"role":"figure","size":93219,"visible":true,"origin":"","legend":"\u003cp\u003ePrincipal component analysis (PCA) of volatile aroma profiles in 12 Lamiaceae species obtained by HS-SPME, showing separation of taxa according to major chemical families.\u003c/p\u003e","description":"","filename":"3.png","url":"https://assets-eu.researchsquare.com/files/rs-8966477/v1/f2954745c3611ebef3b205a7.png"},{"id":105441922,"identity":"b4eb382c-cda1-4107-8801-ac95e9458d83","added_by":"auto","created_at":"2026-03-26 06:12:02","extension":"pdf","order_by":0,"title":"","display":"","copyAsset":false,"role":"manuscript-pdf","size":1877930,"visible":true,"origin":"","legend":"","description":"","filename":"manuscript.pdf","url":"https://assets-eu.researchsquare.com/files/rs-8966477/v1/6635e563-c67e-4440-8e53-45aaed359ed0.pdf"}],"financialInterests":"No competing interests reported.","formattedTitle":"Comparison of Volatile Compounds of Some Medicinal Plants from Lamiaceae Family by HS-SPME Method","fulltext":[{"header":"Introduction","content":"\u003cp\u003eThe Lamiaceae family, comprising 236 genera and 6900 to 7200 species, stands out as one of the most significant herbal families due to its diverse array of medicinal plants [\u003cspan citationid=\"CR1\" class=\"CitationRef\"\u003e1\u003c/span\u003e]. Among the prominent genera with notable medicinal potential are \u003cem\u003eLavandula\u003c/em\u003e, \u003cem\u003eMentha\u003c/em\u003e, \u003cem\u003eMelissa\u003c/em\u003e, \u003cem\u003eOriganum\u003c/em\u003e, \u003cem\u003eRosmarinus\u003c/em\u003e, \u003cem\u003eSalvia\u003c/em\u003e, \u003cem\u003eSideritis\u003c/em\u003e, and \u003cem\u003eThymus\u003c/em\u003e [\u003cspan citationid=\"CR2\" class=\"CitationRef\"\u003e2\u003c/span\u003e]. Lavenders (\u003cem\u003eLavandula\u003c/em\u003e spp.), a standout member of the Lamiaceae family, include more than 39 species distributed across Arabia, the Mediterranean region, Asia, Northern Africa, and the Middle East [\u003cspan citationid=\"CR3\" class=\"CitationRef\"\u003e3\u003c/span\u003e].\u003c/p\u003e \u003cp\u003e \u003cem\u003eLavandula\u003c/em\u003e species are characterized by aromatic compounds such as linalool, α-pinene, limonene, cineole, cis- and trans-ocimene, 3-octanone, camphor, caryophyllene, and terpinene-4-ol (Hajhashemi et al. 2004). \u003cem\u003eLavandula spica\u003c/em\u003e L. and \u003cem\u003eLavandula dentata\u003c/em\u003e L., which are endemic and widely distributed in the Mediterranean part of Turkey, hold special importance. Lavender is in high demand in flavoring, food, and pharmaceutical industries due to its robust aroma [\u003cspan citationid=\"CR4\" class=\"CitationRef\"\u003e4\u003c/span\u003e] A study indicated that the use of lavender oil aromatherapy among individuals diagnosed with fibromyalgia led to a significant enhancement in their quality of life [\u003cspan citationid=\"CR5\" class=\"CitationRef\"\u003e5\u003c/span\u003e].\u003c/p\u003e \u003cp\u003eThe \u003cem\u003eMentha\u003c/em\u003e genus, comprising 18 species, is another famous source of medicinal herbs within the Lamiaceae family. This genus is widely distributed in North America, Europe, Asia, and Africa. Mints are valued for their anti-inflammatory and analgesic properties, making them a valuable tool in folk medicine for addressing various ailments. Among the main species within this genus are \u003cem\u003eMentha spicata\u003c/em\u003e and \u003cem\u003eMentha piperita\u003c/em\u003e L. \u003cem\u003eMentha piperita\u003c/em\u003e L. is a hybrid of \u003cem\u003eM. spicata\u003c/em\u003e and \u003cem\u003eM. aquatic\u003c/em\u003e. The key components extracted from \u003cem\u003eMentha\u003c/em\u003e are identified as menthol, Menthone, and 1,8 cineol [\u003cspan citationid=\"CR6\" class=\"CitationRef\"\u003e6\u003c/span\u003e].\u003c/p\u003e \u003cp\u003eThe \u003cem\u003eMelissa\u003c/em\u003e genus stands out as an aromatic herb within the Lamiaceae family, with its native range encompassing Europe, Asia, southwestern Siberia, and northern Africa. Notably, \u003cem\u003eMelissa Officinalis\u003c/em\u003e L., known as lemon balm, English balm, and sweet balm, is another member of the mint family. Key compounds present in \u003cem\u003eM. Officinalis\u003c/em\u003e L. include citronellol, citral, and linalool [\u003cspan citationid=\"CR7\" class=\"CitationRef\"\u003e7\u003c/span\u003e]. These compounds contribute to its antiviral and antibacterial effects, making it a valuable treatment for ailments caused by viruses and bacteria.\u003c/p\u003e \u003cp\u003e \u003cem\u003eOriganum\u003c/em\u003e genus is a subshrub within the Lamiaceae family, native to Europe, Asia, and North Africa. This genus is pivotal in traditional medicine, particularly in addressing respiratory complaints. With over 18 hybrids and 43 species, \u003cem\u003eOriganum\u003c/em\u003e holds significant diversity [\u003cspan citationid=\"CR8\" class=\"CitationRef\"\u003e8\u003c/span\u003e].\u003c/p\u003e \u003cp\u003e \u003cem\u003eOriganum Majorana\u003c/em\u003e L., \u003cem\u003eOriganum syriacum\u003c/em\u003e var. \u003cem\u003ebevanii\u003c/em\u003e, and \u003cem\u003eOriganum syriacum\u003c/em\u003e L. are endemic species, widely distributed in the Mediterranean region. Notable compounds found in the \u003cem\u003eOriganum\u003c/em\u003e genus include terpinene-4-ol, cis-sabinene, and o-cymene, with their quantities varying among different species [\u003cspan citationid=\"CR9\" class=\"CitationRef\"\u003e9\u003c/span\u003e].\u003c/p\u003e \u003cp\u003e \u003cem\u003eRosmarinus officinalis\u003c/em\u003e L., commonly known as rosemary, is a perennial herbaceous plant renowned for its antioxidant and anti-inflammatory properties which also belongs to the Lamiaceae family and is native to the Mediterranean region. However, due to its valuable culinary and medicinal attributes, it has been widely cultivated across the globe [\u003cspan citationid=\"CR3\" class=\"CitationRef\"\u003e3\u003c/span\u003e]. The versatility of \u003cem\u003eRosmarinus officinalis\u003c/em\u003e L. (rosemary) is evident through its extensive use in the realms of cooking, medicine, and cosmetics. Its robust flavor and aromatic qualities have contributed to its popularity as a culinary ingredient, while its therapeutic potential has been acknowledged for centuries [\u003cspan citationid=\"CR3\" class=\"CitationRef\"\u003e3\u003c/span\u003e]. Beyond its culinary and medicinal roles, rosemary's antibacterial and antifungal attributes have led to its inclusion in aromatherapy, where it is believed to aid in stress reduction and memory enhancement. The compound makeup of rosemary is notably rich in terpenes, including alpha-pinene, beta-pinene, and camphor. These constituents contribute to its distinct properties and applications [\u003cspan citationid=\"CR10\" class=\"CitationRef\"\u003e10\u003c/span\u003e].\u003c/p\u003e \u003cp\u003e \u003cem\u003eSalvia\u003c/em\u003e L., commonly referred to as sage, is a notable genus within the mint family, Lamiaceae. This genus encompasses a diverse array of plants, exceeding 900 species that are distributed globally, primarily in temperate regions. Among the prominent members of the \u003cem\u003eSalvia\u003c/em\u003e genus, \u003cem\u003eSalvia Officinalis\u003c/em\u003e L. holds particular significance. This species boasts a broad spectrum of primary and secondary metabolites, contributing to its valuable medicinal and nutritional attributes. Secondary metabolites in \u003cem\u003eSalvia Officialis\u003c/em\u003e L. include terpenoids, phenolic acids, flavonoids, and tannins. Notably, terpenoids such as thujone, camphor, and cineole are present, each possessing distinct medicinal properties. Thujone, for instance, has been linked to various effects, while camphor and cineole are recognized for their antimicrobial and antifungal properties. These compounds collectively contribute to the diverse therapeutic potential associated with sage [\u003cspan citationid=\"CR11\" class=\"CitationRef\"\u003e11\u003c/span\u003e].\u003c/p\u003e \u003cp\u003e \u003cem\u003eSideritis\u003c/em\u003e spp., commonly referred to as mountain tea, stands as a noteworthy genus of flowering plants within the Lamiaceae family. Indigenous to the Mediterranean region, this genus has gained popularity as an herbal tea. With a substantial presence of over 150 species, \u003cem\u003eSideritis\u003c/em\u003e has a rich history in traditional medicine due to its recognized anti-inflammatory, antioxidant, and antimicrobial attributes. In more recent times, scientific exploration has illuminated the potential of \u003cem\u003eSideritis\u003c/em\u003e as a treatment for Alzheimer's disease and other neurological disorders. This research has underscored its significance beyond traditional applications [\u003cspan citationid=\"CR12\" class=\"CitationRef\"\u003e12\u003c/span\u003e]. The secondary metabolites found within \u003cem\u003eSideritis\u003c/em\u003e spp., notably rosmarinic acid and apigenin, are particularly noteworthy for their significant antioxidant and anti-inflammatory properties. These compounds contribute to the diverse therapeutic potential of \u003cem\u003eSideritis\u003c/em\u003e, making it a valued herbal remedy with potential implications for various health conditions [\u003cspan citationid=\"CR13\" class=\"CitationRef\"\u003e13\u003c/span\u003e].\u003c/p\u003e \u003cp\u003e \u003cem\u003eThymus\u003c/em\u003e L., a perennial shrub belonging to the Lamiaceae family, is more commonly recognized as thyme. Originating in the Mediterranean region, this plant has been cultivated and valued for its aromatic and medicinal attributes over many centuries. Among the various species within this genus, \u003cem\u003eThymus vulgaris\u003c/em\u003e L. stands out, renowned for its remarkable medicinal qualities. This species has earned a prominent place as a natural remedy, addressing an array of health concerns including respiratory infections, digestive troubles, and inflammatory conditions. The therapeutic potential of \u003cem\u003eThymus vulgaris\u003c/em\u003e L. can be attributed to its composition, which is rich in compounds like thymol and carvacrol. These bioactive constituents contribute to the plant's antibacterial, antiviral, and antifungal properties. The presence of these compounds underscores its traditional and contemporary uses as a powerful and versatile herbal remedy [\u003cspan citationid=\"CR14\" class=\"CitationRef\"\u003e14\u003c/span\u003e].\u003c/p\u003e \u003cp\u003eIndeed, the medicinal plant species within the Lamiaceae family hold considerable significance in natural medicine, pharmacology, cosmetology, and aromatherapy due to their diverse secondary metabolites. These include alcohols, aldehydes, ketones, esters, terpenes, and phenolic compounds, which confer antimicrobial, antiviral, antioxidant, and anti-inflammatory activities [15; 16; 17].\u003c/p\u003e \u003cp\u003eDespite extensive studies on essential oils of Lamiaceae species obtained mainly through hydrodistillation, little is known about their volatile composition when analyzed using solvent-free techniques that preserve thermolabile and low-volatility compounds. Moreover, the influence of distinct microclimates on the volatile profiles of these medicinal plants remains underexplored.\u003c/p\u003e \u003cp\u003eTherefore, the novelty of this study lies in applying HS-SPME/GC-MS to comparatively profile the volatiles of 12 medicinal plants collected from two different Turkish provinces (Adana and Osmaniye), thereby addressing the gap in knowledge on how geographical origin affects volatile composition when assessed by this technique.\u003c/p\u003e"},{"header":"Materials and Methods","content":"\u003cdiv id=\"Sec3\" class=\"Section2\"\u003e \u003ch2\u003eMaterial\u003c/h2\u003e \u003cp\u003eTwelve distinct members of the Lamiaceae plant family, including Sweet Marjoram, Lemon Balm, Bible Hyssop, Hybrid Mint, Greek Sage, Lavender, Fringed Lavender, Za'atar, Spearmint, Rosemary, Sage, and Thyme, without undergoing any treatments, were used in the current study. The plant materials were collected from Ali Nihat Gokyigit Botanical Garden (n\u0026thinsp;=\u0026thinsp;7) and Osmaniye (n\u0026thinsp;=\u0026thinsp;5) in July 2019 (Table\u0026nbsp;\u003cspan refid=\"Tab1\" class=\"InternalRef\"\u003e1\u003c/span\u003e). Formal taxonomic identification of the plant material was performed by Dr. Zeynep Ergun based on regional floristic references and morphological characteristics. A voucher specimen of this material was not deposited in publicly accessible herbarium. Following collection, the plant samples were appropriately labeled based on their origin and were subsequently stored at a temperature of -20\u0026deg;C. For subsequent analyses, one gram of each ground plant material.\u003c/p\u003e \u003cp\u003e \u003cdiv class=\"gridtable\"\u003e\u003ctable float=\"Yes\" id=\"Tab1\" border=\"1\"\u003e \u003ccaption language=\"En\"\u003e \u003cdiv class=\"CaptionNumber\"\u003eTable 1\u003c/div\u003e \u003cdiv class=\"CaptionContent\"\u003e \u003cp\u003eStudied twelve different species of Lamiaceae family\u003c/p\u003e \u003c/div\u003e \u003c/caption\u003e \u003ccolgroup cols=\"4\"\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c1\" colnum=\"1\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c2\" colnum=\"2\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c3\" colnum=\"3\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c4\" colnum=\"4\"\u003e\u003c/div\u003e \u003cthead\u003e \u003ctr\u003e \u003cth align=\"left\" colname=\"c1\"\u003e \u003cp\u003eNO\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c2\"\u003e \u003cp\u003eName\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c3\"\u003e \u003cp\u003eSpecies\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c4\"\u003e \u003cp\u003ePlace of Collection\u003c/p\u003e \u003c/th\u003e \u003c/tr\u003e \u003c/thead\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eLavender\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eLavandula Spica\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAdana Botanik Park\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eFringed Lavender or French Lavender,\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eLavandula Dentata\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAdana Botanik Park\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e3\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eLemon Balm\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eMelissa Officinalis\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAdana Botanik Park\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e4\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eSpearmint, Garden Mint, Common Mint, Lamb Mint, Mackerel Mint\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eMentha Spicata\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eOsmaniye\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e5\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eHybrid Mint (Peppermint )\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eMentha Piperita\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eOsmaniye\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eMarjoram\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eOriganum Majorana\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAdana Botanik Park\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e7\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eBible Hyssop, Biblical-Hyssop, Lebanese Oregano, Syrian Oregano\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eOriganum syriacum var. bevanii\u003c/em\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAdana Botanik Park\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e8\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eZa'atar\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eOriganum syriacum\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAdana Botanik Park\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e9\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eRosemary\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eRosmarinus officinalis\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eOsmaniye\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e10\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCommon Sage, Sage\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eSalvia officinalis\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eOsmaniye\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e11\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eGreek Sage\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eSideritis spp.\u003c/em\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAdana Botanik Park\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCommon Thyme, German Thyme, Garden Thyme, Thyme\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e\u003cem\u003eThymus Vulgaris\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003eOsmaniye\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003c/tbody\u003e \u003c/colgroup\u003e \u003c/table\u003e\u003c/div\u003e \u003c/p\u003e \u003c/div\u003e\n\u003ch3\u003eMethods\u003c/h3\u003e\n\u003cdiv id=\"Sec5\" class=\"Section2\"\u003e \u003ch2\u003eHS-SPME extraction of volatile compounds\u003c/h2\u003e \u003cp\u003eVolatile compounds were extracted using the Headspace-Solid Phase Microextraction (HS-SPME) technique. Ground samples were homogenized with 5 M calcium chloride (CaCl₂) to increase ionic strength and facilitate the release of volatile compounds into the headspace, as described in similar extraction protocols [\u003cspan citationid=\"CR18\" class=\"CitationRef\"\u003e18\u003c/span\u003e]. A 100 \u0026micro;m PDMS fiber was employed because it is widely used for monoterpene-rich matrices such as Lamiaceae essential oils. Although a CAR/PDMS fiber was also tested, PDMS fiber yielded a higher number of compounds in our samples, and therefore was selected for subsequent analyses. The fiber was exposed to the sample headspace and incubated for 30 min at 30\u0026deg;C with magnetic stirring. The extraction time was chosen based on preliminary trials showing equilibrium after 30 min, consistent with literatures [\u003cspan citationid=\"CR18\" class=\"CitationRef\"\u003e18\u003c/span\u003e].\u003c/p\u003e \u003c/div\u003e\n\u003ch3\u003eGC/MS analysis\u003c/h3\u003e\n\u003cp\u003eAnalysis was conducted using a Shimadzu GC/MS equipped with a DB-Wax column (30 m \u0026times; 0.25 mm \u0026times; 0.5 \u0026micro;m). Helium was used as the carrier gas at a flow rate of 1.4 mL/min (adjusted to the optimal linear velocity for this column). The oven temperature program started at 40\u0026deg;C, increased at 10\u0026deg;C/min to 200\u0026deg;C (16 min), and was held for 10 min, giving a total run time of ~\u0026thinsp;26 min. This correction addresses a discrepancy in the original text regarding ramp duration. Compound identification was performed tentatively by comparing mass spectra with NIST/Wiley libraries and retention indices. Retention indices were calculated against a C7\u0026ndash;C30 n-alkane series under identical conditions, and reference RI values for DB-Wax were obtained from the NIST database. Quantification was expressed as relative percentage of total ion current (TIC) peak areas, which provides semi-quantitative comparison among samples but does not account for compound-specific ionization efficiencies. All analyses were performed in triplicate. Relative standard deviations (RSD%) were calculated for major compounds to assess analytical precision.\u003c/p\u003e"},{"header":"Result and discussion","content":"\u003cdiv id=\"Sec8\" class=\"Section2\"\u003e \u003ch2\u003eVolatile Compound of Lamiaceae Family\u003c/h2\u003e \u003cp\u003eTable\u0026nbsp;\u003cspan refid=\"Tab2\" class=\"InternalRef\"\u003e2\u003c/span\u003e includes information on the percentage component distribution, retention time, and retention indices for each volatile compound identified in the studied samples. Detected volatile compounds within the Lamiaceae family encompass a diverse array of chemical family groups, comprising 3 volatiles in aldehydes, 23 volatiles in alcohols, 7 volatiles in esters, 3 volatiles in ketones, and 37 volatiles in terpenes. Out of the 74 volatile compounds investigated in this study, terpenes exhibited the widest diversity, while the smallest range was observed in aldehydes (Fig.\u0026nbsp;\u003cspan refid=\"Fig1\" class=\"InternalRef\"\u003e1\u003c/span\u003e). The presence of volatile compounds varied in terms of abundance across different species, ranging from high to low quantities. Additionally, certain compounds were not detected in certain studied species. Terpenes were found to have the highest percentage of volatiles, whereas esters exhibited the lowest percentage. Among the volatile compounds, terpenes emerged as the dominant category for the Lamiaceae family species.\u003c/p\u003e \u003cp\u003e \u003c/p\u003e \u003cp\u003eThe investigation encompassing 12 distinct Lamiaceae species yielded diverse volatile compound profiles. Specifically, \u003cem\u003eLavandula Spica\u003c/em\u003e L. featured 28 volatiles, while \u003cem\u003eLavandula Dentata\u003c/em\u003e L. and \u003cem\u003eMentha Spicata\u003c/em\u003e each contained 23 volatiles. \u003cem\u003eMentha Piperita\u003c/em\u003e L. exhibited 20 volatiles, \u003cem\u003eMelissa Officinalis\u003c/em\u003e L. had 16, and \u003cem\u003eOriganum Majorana\u003c/em\u003e L. had 25. Notably, \u003cem\u003eOriganum syriacum\u003c/em\u003e var. \u003cem\u003ebevanii\u003c/em\u003e showcased 22, while \u003cem\u003eOriganum syriacum\u003c/em\u003e L. and \u003cem\u003eRosmarinus officinalis\u003c/em\u003e L. each featured 21 and 26 volatiles, respectively. \u003cem\u003eSalvia officinalis\u003c/em\u003e L. contained 21 volatiles, \u003cem\u003eSideritis\u003c/em\u003e spp. L. had 18, and \u003cem\u003eThymus Vulgaris\u003c/em\u003e L. featured 24. The most extensive and least extensive species-specific volatile components were observed in \u003cem\u003eLavandula Spica\u003c/em\u003e L. with 28 volatiles and \u003cem\u003eMelissa Officinalis\u003c/em\u003e L. with 16 volatiles, respectively (Table\u0026nbsp;\u003cspan refid=\"Tab2\" class=\"InternalRef\"\u003e2\u003c/span\u003e).\u003c/p\u003e \u003cp\u003e \u003cdiv class=\"gridtable\"\u003e\u003ctable float=\"Yes\" id=\"Tab2\" border=\"1\"\u003e \u003ccaption language=\"En\"\u003e \u003cdiv class=\"CaptionNumber\"\u003eTable 2\u003c/div\u003e \u003cdiv class=\"CaptionContent\"\u003e \u003cp\u003eNumber of Aroma Compounds per Chemical Family in 12 Species of Lamiacea Family.\u003c/p\u003e \u003c/div\u003e \u003c/caption\u003e \u003ccolgroup cols=\"8\"\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c1\" colnum=\"1\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c2\" colnum=\"2\"\u003e\u003c/div\u003e \u003cdiv align=\"char\" char=\".\" class=\"colspec\" colname=\"c3\" colnum=\"3\"\u003e\u003c/div\u003e \u003cdiv align=\"char\" char=\".\" class=\"colspec\" colname=\"c4\" colnum=\"4\"\u003e\u003c/div\u003e \u003cdiv align=\"char\" char=\".\" class=\"colspec\" colname=\"c5\" colnum=\"5\"\u003e\u003c/div\u003e \u003cdiv align=\"char\" char=\".\" class=\"colspec\" colname=\"c6\" colnum=\"6\"\u003e\u003c/div\u003e \u003cdiv align=\"char\" char=\".\" class=\"colspec\" colname=\"c7\" colnum=\"7\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c8\" colnum=\"8\"\u003e\u003c/div\u003e \u003cthead\u003e \u003ctr\u003e \u003cth align=\"left\" colname=\"c1\"\u003e \u003cp\u003eNO\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c2\"\u003e \u003cp\u003eChemical family/Species\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c3\"\u003e \u003cp\u003eAldehydes\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c4\"\u003e \u003cp\u003eAlcohols\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c5\"\u003e \u003cp\u003eEsters\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c6\"\u003e \u003cp\u003eKetones\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colspan=\"2\" nameend=\"c8\" namest=\"c7\"\u003e \u003cp\u003eTerpenes\u003c/p\u003e \u003c/th\u003e \u003c/tr\u003e \u003c/thead\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e1\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eLavandula Spica\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e8\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e18\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e2\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eLavandula Dentata\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e7\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e3\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eMelissa Officinalis\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e4\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eMentha Spicata\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e8\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e3\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e9\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e5\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eMentha Piperita\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e6\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eOriganum Majorana\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e4\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e3\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e16\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e7\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eOriganum syriacum var. bevanii\u003c/em\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e8\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e10\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e8\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eOriganum syriacum\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e9\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e11\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e9\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eRosmarinus officinalis\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e9\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e14\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e10\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eSalvia officinalis\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e5\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e14\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e11\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eSideritis spp.\u003c/em\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e3\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e14\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\"\u003e \u003cp\u003e\u003cb\u003e12\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e\u003cem\u003eThymus Vulgaris\u003c/em\u003e L.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c3\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c4\"\u003e \u003cp\u003e9\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c5\"\u003e \u003cp\u003e2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c6\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"char\" char=\".\" colname=\"c7\"\u003e \u003cp\u003e12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"1\" nameend=\"c8\" namest=\"c8\"\u003e\u0026nbsp;\u003c/td\u003e \u003c/tr\u003e \u003c/tbody\u003e \u003c/colgroup\u003e \u003c/table\u003e\u003c/div\u003e \u003c/p\u003e \u003cp\u003eIn various species of the Lamiaceae family, the terpenes category exhibited notable high-quantity compounds such as eucalyptol, p-cymene, α-thujone, trans-sabinene hydrate, caryophyllene, and β-Pinene. Among the alcohols chemical family, l-(-)-menthol, α-terpineol, 1-Borneol, and Linalool were found in significant quantities. Notably, the esters category was characterized by high quantities of Menthyl acetate and neryl acetate. In terms of aldehydes, citral emerged as a high-quantity compound. Lastly, carvone and camphor stood out as compounds of substantial quantity within the ketones category (Table\u0026nbsp;\u003cspan refid=\"Tab3\" class=\"InternalRef\"\u003e3\u003c/span\u003e).\u003c/p\u003e \u003cp\u003eThis comprehensive study underscores the diverse range of volatile compounds within different Lamiaceae species. Significant percentages of volatile compounds were identified in specific species. For instance, citral from the Aldehyde chemical family was notably present in \u003cem\u003eMelissa Officinalis\u003c/em\u003e L. at a percentage of 65.48%. Among the Alcohols chemical family, L(-)Menthol was detected in \u003cem\u003eMentha Piperita\u003c/em\u003e L. at a level of 33.37%. Menthyl acetate categorized within the Ester chemical family, stood out in \u003cem\u003eMentha Piperita\u003c/em\u003e L. at a level of 30.53%. Within the Ketones chemical family, carvone was identified in \u003cem\u003eMentha Spicata\u003c/em\u003e L. at a percentage of 45.86%. Noteworthy, eucalyptol, a member of the Terpen chemical family, was found in \u003cem\u003eOriganum syriacum\u003c/em\u003e L. at a percentage of 54.71% (Table\u0026nbsp;\u003cspan refid=\"Tab3\" class=\"InternalRef\"\u003e3\u003c/span\u003e).\u003c/p\u003e \u003cp\u003e \u003cdiv class=\"gridtable\"\u003e\u003ctable float=\"Yes\" id=\"Tab3\" border=\"1\"\u003e \u003ccaption language=\"En\"\u003e \u003cdiv class=\"CaptionNumber\"\u003eTable 3\u003c/div\u003e \u003cdiv class=\"CaptionContent\"\u003e \u003cp\u003eVolatile Compound, retention time, retention indices and their percentage composition of studied species of Lamiaceae family.\u003c/p\u003e \u003c/div\u003e \u003c/caption\u003e \u003ccolgroup cols=\"17\"\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c1\" colnum=\"1\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c2\" colnum=\"2\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c3\" colnum=\"3\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c4\" colnum=\"4\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c5\" colnum=\"5\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c6\" colnum=\"6\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c7\" colnum=\"7\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c8\" colnum=\"8\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c9\" colnum=\"9\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c10\" colnum=\"10\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c11\" colnum=\"11\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c12\" colnum=\"12\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c13\" colnum=\"13\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c14\" colnum=\"14\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c15\" colnum=\"15\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c16\" colnum=\"16\"\u003e\u003c/div\u003e \u003cdiv align=\"left\" class=\"colspec\" colname=\"c17\" colnum=\"17\"\u003e\u003c/div\u003e \u003cthead\u003e \u003ctr\u003e \u003cth align=\"left\" colname=\"c1\"\u003e \u003cp\u003eChemical family\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCompounds Name\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c3\"\u003e \u003cp\u003eR.T\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c4\"\u003e \u003cp\u003eRI\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c5\"\u003e \u003cp\u003eDB*-wax\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c6\"\u003e \u003cp\u003e\u003cem\u003e1\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c7\"\u003e \u003cp\u003e\u003cem\u003e2\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c8\"\u003e \u003cp\u003e\u003cem\u003e3\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c9\"\u003e \u003cp\u003e\u003cem\u003e4\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c10\"\u003e \u003cp\u003e\u003cem\u003e5\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c11\"\u003e \u003cp\u003e\u003cem\u003e6\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c12\"\u003e \u003cp\u003e\u003cem\u003e7\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c13\"\u003e \u003cp\u003e\u003cem\u003e8\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c14\"\u003e \u003cp\u003e\u003cem\u003e9\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c15\"\u003e \u003cp\u003e\u003cem\u003e10\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c16\"\u003e \u003cp\u003e\u003cem\u003e11\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003cth align=\"left\" colname=\"c17\"\u003e \u003cp\u003e\u003cem\u003e12\u003c/em\u003e\u003c/p\u003e \u003c/th\u003e \u003c/tr\u003e \u003c/thead\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\" morerows=\"3\" rowspan=\"4\"\u003e \u003cp\u003e\u003cb\u003eAldehyde\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e(E)-2-Hexenal\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e10.05\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1228\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1227\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0.8\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.48\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCitronellal\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e17.40\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1490\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1488\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e0.11\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCitral\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e23.75\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1742\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1741\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e65.48\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e2.47\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e8.29\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e1.52\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e5.2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eTotal Aldehydes\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colspan=\"3\" nameend=\"c5\" namest=\"c3\"\u003e\u0026nbsp;\u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e65.59\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e2.47\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e8.29\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e1.52\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\" morerows=\"22\" rowspan=\"23\"\u003e \u003cp\u003e\u003cb\u003eAlcohols\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e1-Hexanol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e13.69\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1356\u003c/p\u003e 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\u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0.26\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e3-Octanol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e14.86\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1396\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1393\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.96\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e1.6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e1-Octen-3-ol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e16.49\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1458\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1450\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e1.74\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0.36\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e1.84\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e0.08\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e0.6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.39\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e 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colname=\"c7\"\u003e \u003cp\u003e2.21\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.33\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e5.12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e13.91\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0.11\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.19\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e3.88\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e0.06\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e6.44\u003c/p\u003e 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\u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.18\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eMethyleugenol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e30.13\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2029\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2030\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eNerolidol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e30.53\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2049\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2014\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.14\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCarvacrol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e34.03\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2224\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2240\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.18\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.35\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e6.09\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e0.56\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.32\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eVeridiflorol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e31.46\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2093\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2092\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e2.45\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e1.02\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.6\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eSpathulenol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e35.73\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2306\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2129\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.27\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.3\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colspan=\"4\" nameend=\"c5\" namest=\"c2\"\u003e \u003cp\u003eTotal Alcohols\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e10.73\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e25.79\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e5.08\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e1.21\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e38.96\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e23.02\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e5.77\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e10.62\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e31.72\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\" morerows=\"7\" rowspan=\"8\"\u003e \u003cp\u003e\u003cb\u003eEsters\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eMenthyl acetate\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e18.69\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1540\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1541\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e30.53\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0.88\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0.12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e1.34\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e0.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eNeryl acetate\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e23.64\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1738\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1737\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e6.37\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0.17\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.16\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eGeranyl acetate\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e24.36\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1768\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1768\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e0.4\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0.4\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003ep-Cumic aldehyde\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e24.90\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1791\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1794\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e1.79\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eGeranyl propionate\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e25.78\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1829\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1828\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e0.83\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.61\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eEugenol acetate\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e33.17\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2181\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2263\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.75\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eZ-3-hexenyl phenylacetate\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e34.32\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2238\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2220\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.65\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colspan=\"4\" nameend=\"c5\" namest=\"c2\"\u003e \u003cp\u003eTotal Esters\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e8.16\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e1.23\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.75\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0.57\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.65\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\" morerows=\"3\" rowspan=\"4\"\u003e \u003cp\u003e\u003cb\u003eKetones\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCamphor\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e18.20\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1520\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1536\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e15.21\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e29.82\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e1.49\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e13.92\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e17.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.87\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCarvone\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e23.86\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1740\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1744\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e2.38\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e3.44\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e45.86\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e1.38\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003ecis-Jasmone\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e28.13\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1935\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1938\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e1.46\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colspan=\"4\" nameend=\"c5\" namest=\"c2\"\u003e \u003cp\u003eTotal Ketones\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e17.59\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e33.26\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e47.86\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e1.49\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e15.3\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c1\" morerows=\"36\" rowspan=\"37\"\u003e \u003cp\u003e\u003cb\u003eTerpens\u003c/b\u003e\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eα-Pinene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e4.98\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1006\u003c/p\u003e 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\u003cp\u003e6.15\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e14.6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCamphene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e5.85\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1068\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1059\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e1.3\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e 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align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1102\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1096\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e2.6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e3.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.5\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0.7\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e5.13\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e18.09\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eSabinene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e7.05\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1117\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1119\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e1.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.19\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e9.41\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e0.14\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e4.88\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eα-Phellandrene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e8.23\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1162\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1160\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e1.44\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e 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align=\"left\" colname=\"c8\"\u003e \u003cp\u003e23.06\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e3.33\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e1.64\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" 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align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e8.87\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eMenthone\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e16.78\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1492\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1473\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e8.9\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e 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colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e7.35\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e 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align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.51\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e0.28\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e9.08\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.23\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eβ-Bourbonene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e18.36\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1527\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1528\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e1.22\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.68\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.59\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e1.67\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e2.2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e 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align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e0.63\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e3.76\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003e(E)-Pinanone\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e19.00\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1552\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1548\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.2\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e3.56\u003c/p\u003e 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align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0.12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eβ-Elemene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e20.24\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1598\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1599\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.41\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eβ-Guaiene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e20.26\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1599\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1663\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e0.06\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCaryophyllene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e20.37\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1603\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1608\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e2.78\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e8.58\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e2.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e8.75\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e6.72\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e15.88\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e0.7\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e4.62\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e9.82\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e5.65\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eD-Verbenone\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e22.98\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1709\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1723\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e0.27\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e1.1\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e4.94\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eGermacrene D\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e23.23\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1720\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1710\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e1.94\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e10.65\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e2.77\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0.31\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e4.35\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e0.78\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e9.49\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e1.22\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003ePiperitone\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e23.55\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1734\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1735\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e0.87\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e1.64\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e0.7\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.39\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eσ-Cadinene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e24.39\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1769\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1749\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e0.85\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e0.64\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.25\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e5.08\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e3.07\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eα-Calamenene\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e26.12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1845\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1837\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e0.8\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e1.66\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e0.41\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e2.61\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e0.39\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003ePulegone\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e26.63\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1867\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1631\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e2.75\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e0.49\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eThymol\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e33.52\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2198\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2146\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e1.41\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e0.35\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e2.29\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e1.27\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e14.12\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e20.24\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e0.64\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e4.52\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e1.65\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e42.43\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eEstragole\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e22.38\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e1685\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e1685\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e0.99\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e2.46\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e0.34\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e4.34\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colname=\"c2\"\u003e \u003cp\u003eCoumarin\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c3\"\u003e \u003cp\u003e39.95\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c4\"\u003e \u003cp\u003e2459\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c5\"\u003e \u003cp\u003e2458\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e3.22\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e4.35\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003eN.D.\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003ctr\u003e \u003ctd align=\"left\" colspan=\"4\" nameend=\"c5\" namest=\"c2\"\u003e \u003cp\u003eTotal Terpens\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c6\"\u003e \u003cp\u003e69.99\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c7\"\u003e \u003cp\u003e31.6\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c8\"\u003e \u003cp\u003e27.41\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c9\"\u003e \u003cp\u003e45.54\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c10\"\u003e \u003cp\u003e29.8\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c11\"\u003e \u003cp\u003e66.46\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c12\"\u003e \u003cp\u003e90.49\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c13\"\u003e \u003cp\u003e84.82\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c14\"\u003e \u003cp\u003e51.33\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c15\"\u003e \u003cp\u003e77.19\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c16\"\u003e \u003cp\u003e92.06\u003c/p\u003e \u003c/td\u003e \u003ctd align=\"left\" colname=\"c17\"\u003e \u003cp\u003e88.34\u003c/p\u003e \u003c/td\u003e \u003c/tr\u003e \u003c/tbody\u003e \u003c/colgroup\u003e \u003c/table\u003e\u003c/div\u003e \u003c/p\u003e \u003cp\u003eThe heatmap analysis for the aroma profile of 12 species from the Lamiaceae family reveals distinct groupings of species based on their concentrations of specific chemical compounds such as alcohols, aldehydes, esters, ketones, and terpenes (Fig.\u0026nbsp;\u003cspan refid=\"Fig2\" class=\"InternalRef\"\u003e2\u003c/span\u003e). Each species exhibits a unique chemical composition that contributes to its aroma, with several notable patterns emerging from the analysis. \u003cem\u003eMentha\u003c/em\u003e species, including \u003cem\u003eMentha Spicata\u003c/em\u003e L. and \u003cem\u003eMentha Piperita\u003c/em\u003e L., are particularly rich in menthol, menthone, and other related compounds, placing them in a distinct cluster due to their strong minty aroma profiles. On the other hand, \u003cem\u003eMelissa Officinalis\u003c/em\u003e L. stands out with high levels of citral, making it unique among the other species for its lemon-like scent. The presence of high aldehyde concentrations in \u003cem\u003eMelissa Officinalis\u003c/em\u003e L. contrasts with species like \u003cem\u003eLavandula Spica\u003c/em\u003e L. and \u003cem\u003eLavandula Dentata\u003c/em\u003e L., which are rich in linalool and geranyl acetate, compounds that contribute to their sweet and floral scents commonly associated with lavender oils.\u003c/p\u003e \u003cp\u003eThe principal component analysis (PCA) also clearly separated the studied Lamiaceae species based on their volatile compound profiles obtained by HS-SPME. The first two principal components (PC1: 24.9%, PC2: 16.5%) together explained over 40% of the total variance, indicating that a considerable proportion of the chemical variation among species was captured. Samples such as \u003cem\u003eOriganum syriacum\u003c/em\u003e and \u003cem\u003eLavandula stoechas\u003c/em\u003e were distinctly positioned along PC1, largely influenced by high contributions from terpenes and ketones, while \u003cem\u003eMelissa officinalis\u003c/em\u003e and \u003cem\u003eMentha spicata\u003c/em\u003e clustered closer together, reflecting their higher alcohol contents. The strong loadings of compounds such as linalool, geraniol, and camphor suggest that these metabolites were the main drivers of separation among species. The PCA biplot therefore highlights the chemical diversity of Lamiaceae volatiles and demonstrates that terpenes and alcohols are the most discriminative chemical families. This chemometric approach provides a clear comparative framework, enabling differentiation of closely related taxa based on their volatile fingerprints (Fig.\u0026nbsp;\u003cspan refid=\"Fig3\" class=\"InternalRef\"\u003e3\u003c/span\u003e).\u003c/p\u003e \u003cp\u003e \u003c/p\u003e \u003cp\u003e \u003c/p\u003e \u003cp\u003eTerpenes such as thymol, carvacrol, and eucalyptol are prominent in species like \u003cem\u003eThymus Vulgaris\u003c/em\u003e L., \u003cem\u003eOriganum syriacum\u003c/em\u003e L., and \u003cem\u003eRosmarinus officinalis\u003c/em\u003e L., which group together due to their strong herbal and camphoraceous aromas, making them valuable in medicinal and antiseptic applications. The dendrogram included in the heatmap illustrates these relationships by clustering species that share similar concentrations of these key compounds. For example, the close clustering of \u003cem\u003eOriganum Majorana\u003c/em\u003e L. and \u003cem\u003eOriganum syriacum\u003c/em\u003e L. reflects their similar terpene profiles, while species like \u003cem\u003eSideritis\u003c/em\u003e spp. and \u003cem\u003eSalvia officinalis\u003c/em\u003e L. form another cluster based on their diverse chemical makeup, particularly in terms of their high terpene content.\u003c/p\u003e \u003cp\u003eThe clustering of species based on their chemical profiles helps to identify potential uses for each plant. For instance, species high in alcohols like Linalool (e.g., lavender species) are ideal for perfumery, while those rich in menthol and menthone (e.g., mint species) are suitable for medicinal and culinary purposes. The high terpene concentrations in species like \u003cem\u003eThymus Vulgaris\u003c/em\u003e L. and \u003cem\u003eOriganum syriacum\u003c/em\u003e L. highlight their antimicrobial and antifungal properties, making them valuable for therapeutic use. Overall, this heatmap analysis underscores the chemical diversity within the Lamiaceae family and provides a comprehensive framework for understanding how different species can be clustered based on their aroma profiles for various applications.\u003c/p\u003e \u003c/div\u003e\n\u003ch3\u003eVariation of volatile compounds among plant species\u003c/h3\u003e\n\u003cp\u003eThe analysis of aromatic compounds within the Lamiaceae family has unveiled a diverse range of constituents that significantly contribute to their distinct scent profiles and potential therapeutic attributes. Within \u003cem\u003eLavandula Spica\u003c/em\u003e L., Eucalyptol emerges as a prominent element, constituting a significant portion (41.29%) alongside Camphor (15.21%). Eucalyptol carries a refreshing, camphor-like fragrance with a hint of peppery coolness. Its alluring aromatic and flavor qualities make it valuable in fragrances, cosmetics, and as a flavor enhancer. Eucalyptol has demonstrated antinociceptive properties, suggesting potential calming and central nervous system depressant effects [\u003cspan citationid=\"CR19\" class=\"CitationRef\"\u003e19\u003c/span\u003e]. Inhalation of eucalyptus aromatherapy oil, abundant in over 80% eucalyptol, has proven effective in mitigating post-COVID syndrome symptoms, such as breathlessness, back pain, and anxiety affecting individuals worldwide and potentially bearing labor and financial repercussions [\u003cspan citationid=\"CR5\" class=\"CitationRef\"\u003e5\u003c/span\u003e]. Furthermore, the therapeutic potential of eucalyptol spans cardiovascular treatments, antimicrobial effects, anti-inflammatory benefits, and respiratory disorder support, corroborated by numerous studies [\u003cspan citationid=\"CR1\" class=\"CitationRef\"\u003e1\u003c/span\u003e]. Conversely, Eucalyptol remains undetected in \u003cem\u003eLavandula Dentata\u003c/em\u003e L., where Camphor (29.82%), Caryophyllene (8.58%), 1-Borneol (8.4%), and Neryl acetate (6.37%) emerge as primary volatile compounds. The prevalence of camphor-rich compounds in \u003cem\u003eLavandula\u003c/em\u003e species is validated by multiple scientific publications [\u003cspan citationid=\"CR20\" class=\"CitationRef\"\u003e20\u003c/span\u003e]. However, some researchers have reported linalool as the principal compound in the essential oil of \u003cem\u003eLavandula\u003c/em\u003e species [\u003cspan citationid=\"CR21\" class=\"CitationRef\"\u003e21\u003c/span\u003e]. Both Camphor and 1-Borneol have demonstrated extensive and diverse pharmacological effects, encompassing anti-inflammatory, analgesic, and antipyretic properties and notable antimicrobial activity [\u003cspan citationid=\"CR22\" class=\"CitationRef\"\u003e22\u003c/span\u003e].\u003c/p\u003e \u003cp\u003e \u003cem\u003eMelissa Officinalis\u003c/em\u003e L. exhibited a notable abundance of Citral (65.48%) and β-Myrcene (23.06%). Previous studies have documented the presence of Citral in \u003cem\u003eMelissa\u003c/em\u003e species [\u003cspan citationid=\"CR23\" class=\"CitationRef\"\u003e23\u003c/span\u003e], while the occurrence of β-Myrcene was initially observed in this study. Myrcene finds application in cosmetics, soaps, detergents, and as a versatile food additive. It also holds a foundational role in creating essential fragrances such as menthol, citral, citronellol, and others, which are pivotal in the production of commercially significant compounds. Several studies have also revealed the properties of β-Myrcene, encompassing anxiolytic, antioxidant, anti-aging, anti-inflammatory, and analgesic attributes [\u003cspan citationid=\"CR24\" class=\"CitationRef\"\u003e24\u003c/span\u003e].\u003c/p\u003e \u003cp\u003eThe dominant volatile compounds in \u003cem\u003eMentha Spicata\u003c/em\u003e L. were Carvone (45.86%) and eucalyptol (16.27%). On the other hand, the primary volatile compounds in \u003cem\u003eMentha Piperita\u003c/em\u003e L. consisted of L-(-)-Menthol (33.37%), Menthyl acetate (30.53%), Menthone (8.9%) and Eucalyptol (6.31%).\u003c/p\u003e \u003cp\u003eThe investigation by Park et al. [\u003cspan citationid=\"CR25\" class=\"CitationRef\"\u003e25\u003c/span\u003e] reported eucalyptol (46.28\u0026thinsp;\u0026plusmn;\u0026thinsp;4.25), caryophyllene (5.47\u0026thinsp;\u0026plusmn;\u0026thinsp;0.49), and menthol (3.02\u0026thinsp;\u0026plusmn;\u0026thinsp;0.22) as the major components in \u003cem\u003eMentha spp\u003c/em\u003e, which are quite similar to the volatile compounds identified in the present study, although caryophyllene was found at a higher level in our results.\u003c/p\u003e \u003cp\u003eIn the current study, the highlighted volatile compounds of three \u003cem\u003eOriganum\u003c/em\u003e species; \u003cem\u003eOriganum Majorana\u003c/em\u003e L., \u003cem\u003eOriganum syriacum\u003c/em\u003e L., and \u003cem\u003eOriganum syriacum\u003c/em\u003e var. bevanii comprised trans sabinene hydrate (30.63%), eucalyptol (54.71%), p-cymene (36.21%), respectively. Terpenes have consistently emerged as the key active components in Oregano species [\u003cspan citationid=\"CR26\" class=\"CitationRef\"\u003e26\u003c/span\u003e]. \u003cem\u003eRosmarinus officinalis\u003c/em\u003e L. exhibited α-Terpineol (22.19%), camphor (13.92%), and eucalyptol (22.42%) as its primary compounds. This study marks the first time identification of α-Terpineol and eucalyptol in this context. \u003cem\u003eSalvia officinalis\u003c/em\u003e L. featured α-thujone (30.97%) and camphor (17.54%), as its prominent volatile compounds. In the case of \u003cem\u003eSideritis\u003c/em\u003e spp., the major component was β-pinene (18.09%), differing from the observations of Kardali et al. [\u003cspan citationid=\"CR27\" class=\"CitationRef\"\u003e27\u003c/span\u003e] which α-pinene was the primary compound. \u003cem\u003eThymus Vulgaris\u003c/em\u003e L. demonstrated richness in thymol (42.43%) and p-cymene (27.6%).\u003c/p\u003e \u003cp\u003eThe species of Lamiaceae family for this study were collected from two distinct locations, Adana Botanik Park and Osmaniye, providing insight into the contrasting climate of these regions. The discernible differences in weather patterns and climatic attributes reflect the distinctive conditions between Osmaniye and Adana. Osmaniye in southern Turkey exhibits a Mediterranean climate characterized by hot, dry summers and moderate, wet winters. Meanwhile, Adana, located nearby, shares a Mediterranean climate but tends to be slightly warmer and more arid due to its lower elevation and proximity to the Mediterranean Sea. This results in Adana often having warmer summertime temperatures and receiving less precipitation compared to Osmaniye. Despite the overall similarity in climate, these subtle variations in temperature and rainfall underscore the existence of microclimatic nuances, even within close proximity. These factors contribute significantly to the substantial differences observed in the compounds in the current study. According to the literature review, variations in volatile compounds are influenced by factors such as location, seasonal changes, and developmental stages [28; 29].\u003c/p\u003e"},{"header":"Conclusion","content":"\u003cp\u003eThe Lamiaceae family includes numerous species widely used in traditional medicine. In this study, twelve species collected from Adana and Osmaniye (Turkey) exhibited diverse volatile profiles comprising aldehydes, alcohols, esters, ketones, and terpenes. Among these, terpenes were the dominant chemical group across all species, consistent with previous essential oil studies. Unlike many earlier works that applied hydrodistillation, our study utilized HS-SPME/GC-MS, which allowed detection of thermolabile and low-volatility compounds that are often lost during conventional extraction. This represents one of the first comparative HS-SPME-based surveys of multiple Lamiaceae species grown under different microclimatic conditions. The comparative results demonstrated that plants collected from Osmaniye were relatively richer in aldehydes, alcohols, and esters, whereas plants from Adana contained higher levels of ketones and terpenes. These findings highlight the significant influence of local microclimatic factors on volatile composition, an aspect rarely considered in previous research. It is important to note that the compounds were tentatively identified based on library matching and retention indices, and quantification was semi-quantitative. Therefore, results should be interpreted as relative rather than absolute concentrations. Future work should validate major compounds using pure standards, apply mixed-phase SPME fibers for broader coverage, and integrate chemometric tools (PCA, cluster analysis) to better resolve interspecies differences. Overall, this study contributes new insights into the volatile diversity of Lamiaceae species under different Turkish microclimates and demonstrates the utility of HS-SPME/GC-MS as a complementary approach to hydrodistillation. These results may support future standardization of medicinal plant products and guide cultivation strategies aimed at optimizing the yield of bioactive volatile constituents.\u003c/p\u003e"},{"header":"Abbreviations","content":"\u003cp\u003eAll abbreviations used in this manuscript are defined and presented in the table below:\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eHS-SPME\u003c/strong\u003e: Headspace Solid-Phase Microextraction\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eGC-MS\u003c/strong\u003e: Gas Chromatography-Mass Spectrometry\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003e\u003cem\u003eM. spicata\u003c/em\u003e\u003c/strong\u003e\u003cem\u003e: Mentha spicata\u003c/em\u003e\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003e\u003cem\u003eM. piperita L.\u003c/em\u003e\u003c/strong\u003e\u003cem\u003e: Mentha piperita\u003c/em\u003e L.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003e\u003cem\u003eM. Officinalis L\u003c/em\u003e\u003c/strong\u003e\u003cem\u003e.: Melissa officinalis\u003c/em\u003e L.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003e\u003cem\u003eSideritis spp\u003c/em\u003e\u003c/strong\u003e\u003cem\u003e.: Sideritis\u003c/em\u003e species\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eTIC\u003c/strong\u003e: Total Ion Current\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eRSD%\u003c/strong\u003e: Relative Standard Deviation (percentage)\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003ePDMS\u003c/strong\u003e: Polydimethylsiloxane\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eCAR\u003c/strong\u003e: Carboxen\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eNIST\u003c/strong\u003e: National Institute of Standards and Technology\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eRI\u003c/strong\u003e: Retention Index\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003ePCA\u003c/strong\u003e: Principal Component Analysis\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003ePC\u003c/strong\u003e: Principal Component\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eSpp\u003c/strong\u003e.: Species\u0026nbsp;\u003c/p\u003e"},{"header":"Declarations","content":"\u003cp\u003e\u003cstrong\u003eEthics Approval and Consent to Participate\u003c/strong\u003e\u003c/p\u003e\n\u003cp\u003eThis study was conducted in full compliance with ethical principles, ensuring the protection of participants' rights and welfare throughout the research process. The study adhered to established ethical guidelines, and informed and voluntary consent was obtained from all participants prior to their involvement in the study.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eConsent for Publication\u003c/strong\u003e\u003c/p\u003e\n\u003cp\u003eThis manuscript includes identifiable information of the authors (such as names and affiliations), but it does not include any identifiable information of participants (such as images, faces, or other personal data). Therefore, the \"Consent for Publication\" section is \"NOT APPLICABLE\" for this manuscript.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eAvailability of Data and Materials\u003c/strong\u003e\u003c/p\u003e\n\u003cp\u003eAll data and materials utilized in this research are available upon request. For access to the dataset or research materials, please contact the corresponding author.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eCompeting Interests\u003c/strong\u003e\u003c/p\u003e\n\u003cp\u003eThe authors declare that they have no financial or non-financial competing interests related to this research. There is no conflict of interest in the conduct or reporting of this study.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eFunding\u003c/strong\u003e\u003c/p\u003e\n\u003cp\u003eThis research was not funded by any external organizations. The authors self-financed the study and the associated research activities.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eAuthors' Contributions\u003c/strong\u003e\u003c/p\u003e\n\u003cp\u003eEach author has contributed significantly to the conception, design, data analysis, writing, and revision of the manuscript. The corresponding author, (name of corresponding author), supervised the submission process and coordinated revisions.\u003c/p\u003e\n\u003cp\u003e\u003cstrong\u003eAcknowledgements\u003c/strong\u003e\u003c/p\u003e\n\u003cp\u003eThe authors would like to express their gratitude for the scientific and technical support provided by the universities associated with the authors, which greatly facilitated the completion of this research.\u003c/p\u003e"},{"header":"References","content":"\u003col\u003e\u003cli\u003e\u003cspan\u003eFidan H, Stankov S, Ivanova T, Stoyanova A, Damyanova S, Ercisli S. Characterization of aromatic compounds and antimicrobial properties of four spice essential oils from family Lamiaceae. Ukr Food J. 2019;8(2):227\u0026ndash;38.\u003c/span\u003e\u003c/li\u003e \u003cli\u003e\u003cspan\u003eBekut M, Brkić S, Kladar N, Dragović G, Gavarić N, Božin B. Potential of selected Lamiaceae plants in anti-(retro)viral therapy. 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The influence of harvest time on essential oil composition, phenolic constituents, and antioxidant properties of Turkish oregano (\u003cem\u003eOriganum onites\u003c/em\u003e L). J Sci Food Agric. 2010;90(2):205\u0026ndash;9.\u003c/span\u003e\u003c/li\u003e \u003cli\u003e\u003cspan\u003eKardali MO, Velasco-Negueruela A, Alonso MP. Essential oil constituents of \u003cem\u003eSideritis ibanyezii\u003c/em\u003e Pau. Bot Complut. 2000;24:101\u0026ndash;6.\u003c/span\u003e\u003c/li\u003e \u003cli\u003e\u003cspan\u003e\u0026Uuml;\u0026ccedil;\u0026uuml;nc\u0026uuml;oğlu D, Sivri-\u0026Ouml;zay D. Geographical origin impact on volatile composition and some quality parameters of virgin olive oils extracted from the Ayvalık variety. Heliyon. 2020;6(9):e04987.\u003c/span\u003e\u003c/li\u003e \u003cli\u003e\u003cspan\u003eDursun A, \u0026Ccedil;alışkan O, G\u0026uuml;ler Z, Bayazit S, T\u0026uuml;rkmen D, G\u0026uuml;nd\u0026uuml;z K. Effect of harvest maturity on volatile compounds profiling and eating quality of hawthorn (\u003cem\u003eCrataegus azarolus\u003c/em\u003e L.) fruit. Sci Hortic. 2021;288:110398.\u003c/span\u003e\u003c/li\u003e\u003c/ol\u003e"}],"fulltextSource":"","fullText":"","funders":[],"hasAdminPriorityOnWorkflow":false,"hasManuscriptDocX":true,"hasOptedInToPreprint":true,"hasPassedJournalQc":"","hasAnyPriority":false,"hideJournal":true,"highlight":"","institution":"","isAcceptedByJournal":false,"isAuthorSuppliedPdf":false,"isDeskRejected":"","isHiddenFromSearch":false,"isInQc":false,"isInWorkflow":false,"isPdf":false,"isPdfUpToDate":true,"isWithdrawnOrRetracted":false,"journal":{"display":true,"email":"[email protected]","identity":"researchsquare","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":true,"externalIdentity":"","sideBox":"","snPcode":"","submissionUrl":"/submission","title":"Research Square","twitterHandle":"researchsquare","acdcEnabled":true,"dfaEnabled":false,"editorialSystem":"","reportingPortfolio":"","inReviewEnabled":false,"inReviewRevisionsEnabled":true},"keywords":"Lamiaceae, Medicinal Plant, Volatile compounds, HS-SPME, GC–MS","lastPublishedDoi":"10.21203/rs.3.rs-8966477/v1","lastPublishedDoiUrl":"https://doi.org/10.21203/rs.3.rs-8966477/v1","license":{"name":"CC BY 4.0","url":"https://creativecommons.org/licenses/by/4.0/"},"manuscriptAbstract":"\u003cp\u003eThis study investigates the volatile compounds in twelve medicinal plants from the Lamiaceae family using headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry (HS-SPME/GC-MS). Lamiaceae plants are recognized for their diverse medicinal properties, including antioxidative, antibacterial, and antifungal effects. A total of 74 volatile compounds were identified, encompassing terpenes, alcohols, esters, aldehydes, and ketones. Notably, \u003cem\u003eLavandula spica\u003c/em\u003e L. exhibited the highest number of unique volatiles (28), while Melissa officinalis L. had the fewest (16). Key compounds included Citral (65.48%) in \u003cem\u003eMelissa officinalis\u003c/em\u003e L., Menthol (33.37%) and \u003cem\u003eMenthyl acetate\u003c/em\u003e (30.53%) in \u003cem\u003eMentha piperita\u003c/em\u003e L., Carvone (45.86%) in \u003cem\u003eMentha spicata\u003c/em\u003e L., and Eucalyptol (54.71%) in \u003cem\u003eOriganum syriacum\u003c/em\u003e L. Plants from Adana Botanic Park were rich in terpenes and ketones, whereas those from Osmaniye contained higher levels of alcohols, aldehydes, and esters. The findings emphasize the impact of geographic location on volatile profiles and suggest avenues for further research into medicinal efficacy and optimal dosage.\u003c/p\u003e","manuscriptTitle":"Comparison of Volatile Compounds of Some Medicinal Plants from Lamiaceae Family by HS-SPME Method","msid":"","msnumber":"","nonDraftVersions":[{"code":1,"date":"2026-03-09 16:15:40","doi":"10.21203/rs.3.rs-8966477/v1","editorialEvents":[{"type":"communityComments","content":0}],"status":"published","journal":{"display":true,"email":"[email protected]","identity":"researchsquare","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":true,"externalIdentity":"","sideBox":"","snPcode":"","submissionUrl":"/submission","title":"Research Square","twitterHandle":"researchsquare","acdcEnabled":true,"dfaEnabled":false,"editorialSystem":"","reportingPortfolio":"","inReviewEnabled":false,"inReviewRevisionsEnabled":true}}],"origin":"","ownerIdentity":"9c10eafe-93ee-4a67-9ada-aab953cc6fa8","owner":[],"postedDate":"March 9th, 2026","published":true,"recentEditorialEvents":[],"rejectedJournal":[],"revision":"","amendment":"","status":"posted","subjectAreas":[],"tags":[],"updatedAt":"2026-03-26T06:11:10+00:00","versionOfRecord":[],"versionCreatedAt":"2026-03-09 16:15:40","video":"","vorDoi":"","vorDoiUrl":"","workflowStages":[]},"version":"v1","identity":"rs-8966477","journalConfig":"researchsquare"},"__N_SSP":true},"page":"/article/[identity]/[[...version]]","query":{"redirect":"/article/rs-8966477","identity":"rs-8966477","version":["v1"]},"buildId":"XKTyCvWXoU3ODBz1xrDgd","isFallback":false,"isExperimentalCompile":false,"dynamicIds":[84888],"gssp":true,"scriptLoader":[]}