Novel Hierarchical Structure of MoS2/TiO2/Ti3C2Tx Composites for Dramatically Enhanced Electromagnetic Absorbing Properties

Novel Hierarchical Structure of MoS2/TiO2/Ti3C2Tx Composites for Dramatically Enhanced Electromagnetic Absorbing Properties | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Novel Hierarchical Structure of MoS 2 /TiO 2 /Ti 3 C 2 T x Composites for Dramatically Enhanced Electromagnetic Absorbing Properties Heng Du, Qipeng Zhang, Biao Zhao, Frank Marken, Qiancheng Gao, and 7 more This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-184920/v1 This work is licensed under a CC BY 4.0 License Status: Under Review Version 1 posted 12 You are reading this latest preprint version Abstract In order to prevent the microwave leakage and mutual interference, more and more microwave absorbing devices are added into the design of electronic products to ensure its routine operation. In this work, we have successfully prepared MoS 2 /TiO 2 /Ti 3 C 2 T x hierarchical composites by one-pot hydrothermal method and focused on the relationship between structures and electromagnetic absorbing properties. Supported by comprehensive characterizations, MoS 2 nanosheets were proved to be anchored on the surface and interlayer of Ti 3 C 2 T x through a hydrothermal process. Additionally, TiO 2 nanoparticles were obtained in situ. Due to these hierarchical structures, the MoS 2 /TiO 2 /Ti 3 C 2 T x composites showed greatly enhanced microwave absorbing performance. The MoS 2 /TiO 2 /Ti 3 C 2 Tx composites exhibit a maximum reflection loss value of −33.5 dB at 10.24 GHz and the effective absorption bandwidth covers 3.1 GHz (13.9–17 GHz) at the thickness of 1.0 mm, implying the features of wide frequency and light weight. This work in the hierarchical structure MoS 2 /TiO 2 /Ti 3 C 2 T x composites opens a promising door to the exploration of constructing extraordinary electromagnetic wave absorbents. Ceramics MoS2/TiO2/Ti3C2Tx hierarchical hybrids Microwave absorbing properties dielectric loss Figures Figure 1 Figure 2 Figure 3 Figure 4 Figure 5 Figure 6 Figure 7 Figure 8 Figure 9 Figure 10 Full Text Cite Share Download PDF Status: Under Review Version 1 posted Review # 3 received at journal 02 Mar, 2021 Editorial decision: Major revisions 02 Mar, 2021 Review # 2 received at journal 22 Feb, 2021 Reviewer # 3 agreed at journal 16 Feb, 2021 Reviewer # 2 agreed at journal 13 Feb, 2021 Reviewer # 1 agreed at journal 28 Jan, 2021 Review # 1 received at journal 28 Jan, 2021 Reviewers invited by journal 27 Jan, 2021 Editor assigned by journal 26 Jan, 2021 Submission checks completed at journal 26 Jan, 2021 Editor invited by journal 26 Jan, 2021 First submitted to journal 25 Jan, 2021 You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. 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Also discoverable on Platform About Our Team In Review Editorial Policies Advisory Board Help Center Resources Author Services Accessibility API Access RSS feed Manage Cookie Preferences © Research Square 2026 | ISSN 2693-5015 (online) Privacy Policy Terms of Service Do Not Sell My Personal Information {"props":{"pageProps":{"initialData":{"identity":"rs-184920","acceptedTermsAndConditions":true,"allowDirectSubmit":false,"archivedVersions":[],"articleType":"Research Article","associatedPublications":[],"authors":[{"id":9598771,"identity":"a6dee064-9bd6-4ed2-a483-0b43490b0d6d","order_by":0,"name":"Heng Du","email":"","orcid":"","institution":"Zhengzhou University","correspondingAuthor":false,"submittingAuthor":false,"prefix":"","firstName":"Heng","middleName":"","lastName":"Du","suffix":""},{"id":9598772,"identity":"52eb30b2-855a-4e67-9763-c6847b2e67ab","order_by":1,"name":"Qipeng Zhang","email":"","orcid":"","institution":"Zhengzhou 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","description":"","filename":"OnlineFig.7.png","url":"https://assets-eu.researchsquare.com/files/rs-184920/v1/abe8a42cd1584c0017d28ccc.png"},{"id":5838604,"identity":"90746f7d-5100-49e0-8c9b-63c9d1ecf136","added_by":"auto","created_at":"2021-02-10 19:41:34","extension":"png","order_by":8,"title":"Figure 8","display":"","copyAsset":false,"role":"figure","size":44508,"visible":true,"origin":"","legend":"Cole–Cole curves of MoS2/TiO2/Ti3C2Tx composites (S2) samples","description":"","filename":"OnlineFig.8.png","url":"https://assets-eu.researchsquare.com/files/rs-184920/v1/e9c1dc4899164ec6e0a49f29.png"},{"id":5838606,"identity":"3e5f339b-9055-4e30-8adc-45a460a8e43e","added_by":"auto","created_at":"2021-02-10 19:41:34","extension":"png","order_by":9,"title":"Figure 9","display":"","copyAsset":false,"role":"figure","size":219789,"visible":true,"origin":"","legend":"Reflection loss curves of MoS2(a) and MoS2/TiO2/Ti3C2Tx composites (b: S1; c: S2; d: S3) with different thickness.","description":"","filename":"OnlineFig.9.png","url":"https://assets-eu.researchsquare.com/files/rs-184920/v1/32e560ced54110f353c2ae44.png"},{"id":5838607,"identity":"553ab602-885f-4069-a6ec-3530a530f899","added_by":"auto","created_at":"2021-02-10 19:41:34","extension":"jpg","order_by":10,"title":"Figure 10","display":"","copyAsset":false,"role":"figure","size":348895,"visible":true,"origin":"","legend":"Diagrammatic drawing of the electromagnetic wave absorption mechanism of the MoS2/TiO2/Ti3C2Tx composites","description":"","filename":"Fig.10.jpg","url":"https://assets-eu.researchsquare.com/files/rs-184920/v1/5fcafa1ee1d46d7a1a0c4105.jpg"},{"id":13582913,"identity":"bbf70518-a280-41ff-a260-d733eeb5b64c","added_by":"auto","created_at":"2021-09-17 04:33:03","extension":"pdf","order_by":1,"title":"","display":"","copyAsset":false,"role":"manuscript-pdf","size":1747075,"visible":true,"origin":"","legend":"","description":"","filename":"2021.01.25FMtextwithoutendnote.pdf","url":"https://assets-eu.researchsquare.com/files/rs-184920/v1_covered.pdf"},{"id":5839378,"identity":"d96faa1d-e28d-43b4-96a9-cee8f1e9db32","added_by":"auto","created_at":"2021-02-10 19:50:38","extension":"pdf","order_by":1,"title":"","display":"","copyAsset":false,"role":"manuscript-pdf","size":602152,"visible":true,"origin":"","legend":"","description":"","filename":"2021.01.25FMtextwithoutendnote.pdf","url":"https://assets-eu.researchsquare.com/files/rs-184920/v1_stamped.pdf"}],"financialInterests":"","formattedTitle":"\u003cp\u003eNovel Hierarchical Structure of MoS\u003csub\u003e2\u003c/sub\u003e/TiO\u003csub\u003e2\u003c/sub\u003e/Ti\u003csub\u003e3\u003c/sub\u003eC\u003csub\u003e2\u003c/sub\u003eT\u003csub\u003ex\u0026nbsp;\u003c/sub\u003eComposites for Dramatically Enhanced Electromagnetic Absorbing Properties\u003c/p\u003e","fulltext":[{"header":"Full Text","content":"\u003cp\u003eThis preprint is available for \u003ca href='/article/rs-184920/latest.pdf' target='_blank'\u003edownload as a PDF\u003c/a\u003e.\u003c/p\u003e"}],"fulltextSource":"","fullText":"","funders":[],"hasAdminPriorityOnWorkflow":false,"hasManuscriptDocX":false,"hasOptedInToPreprint":true,"hasPassedJournalQc":"","hasAnyPriority":false,"hideJournal":false,"highlight":"","institution":"","isAcceptedByJournal":true,"isAuthorSuppliedPdf":true,"isDeskRejected":"","isHiddenFromSearch":false,"isInQc":false,"isInWorkflow":true,"isPdf":false,"isPdfUpToDate":true,"isWithdrawnOrRetracted":false,"journal":{"display":true,"email":"[email protected]","identity":"journal-of-advanced-ceramics","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":false,"externalIdentity":"jace","sideBox":"Learn more about [Journal of Advanced Ceramics](http://link.springer.com/journal/40145)","snPcode":"","submissionUrl":"https://www.editorialmanager.com/jace/default.aspx","title":"Journal of Advanced Ceramics","twitterHandle":"","acdcEnabled":true,"dfaEnabled":false,"editorialSystem":"em","reportingPortfolio":"BMC/SO AJ","inReviewEnabled":true,"inReviewRevisionsEnabled":true},"keywords":"MoS2/TiO2/Ti3C2Tx hierarchical hybrids, Microwave absorbing properties, dielectric loss","lastPublishedDoi":"10.21203/rs.3.rs-184920/v1","lastPublishedDoiUrl":"https://doi.org/10.21203/rs.3.rs-184920/v1","license":{"name":"CC BY 4.0","url":"https://creativecommons.org/licenses/by/4.0/"},"manuscriptAbstract":"\u003cp\u003eIn order to prevent the microwave leakage and mutual interference, more and more microwave absorbing devices are added into the design of electronic products to ensure its routine operation. In this work, we have successfully prepared MoS\u003csub\u003e2\u003c/sub\u003e/TiO\u003csub\u003e2\u003c/sub\u003e/Ti\u003csub\u003e3\u003c/sub\u003eC\u003csub\u003e2\u003c/sub\u003eT\u003csub\u003ex\u003c/sub\u003e hierarchical composites by one-pot hydrothermal method and focused on the relationship between structures and electromagnetic absorbing properties. Supported by comprehensive characterizations, MoS\u003csub\u003e2\u003c/sub\u003e nanosheets were proved to be anchored on the surface and interlayer of Ti\u003csub\u003e3\u003c/sub\u003eC\u003csub\u003e2\u003c/sub\u003eT\u003csub\u003ex\u003c/sub\u003e through a hydrothermal process. Additionally, TiO\u003csub\u003e2\u003c/sub\u003e nanoparticles were obtained in situ. Due to these hierarchical structures, the MoS\u003csub\u003e2\u003c/sub\u003e/TiO\u003csub\u003e2\u003c/sub\u003e/Ti\u003csub\u003e3\u003c/sub\u003eC\u003csub\u003e2\u003c/sub\u003eT\u003csub\u003ex\u003c/sub\u003e composites showed greatly enhanced microwave absorbing performance. The MoS\u003csub\u003e2\u003c/sub\u003e/TiO\u003csub\u003e2\u003c/sub\u003e/Ti\u003csub\u003e3\u003c/sub\u003eC\u003csub\u003e2\u003c/sub\u003eTx composites exhibit a maximum reflection loss value of −33.5 dB at 10.24 GHz and the effective absorption bandwidth covers 3.1 GHz (13.9–17 GHz) at the thickness of 1.0 mm, implying the features of wide frequency and light weight. This work in the hierarchical structure MoS\u003csub\u003e2\u003c/sub\u003e/TiO\u003csub\u003e2\u003c/sub\u003e/Ti\u003csub\u003e3\u003c/sub\u003eC\u003csub\u003e2\u003c/sub\u003eT\u003csub\u003ex \u003c/sub\u003ecomposites opens a promising door to the exploration of constructing extraordinary electromagnetic wave absorbents.\u003c/p\u003e","manuscriptTitle":"Novel Hierarchical Structure of MoS2/TiO2/Ti3C2Tx\u0026nbsp;Composites for Dramatically Enhanced Electromagnetic Absorbing Properties","msid":"","msnumber":"","nonDraftVersions":[{"code":1,"date":"2021-02-10 19:38:32","doi":"10.21203/rs.3.rs-184920/v1","editorialEvents":[{"type":"communityComments","content":0},{"type":"editorInvitedReview","content":"","date":"2021-03-03T00:00:00+00:00","index":3,"fulltext":"Recommendation: Reviewer's comments unavailable due to the journal's policy.\n"},{"type":"decision","content":"Major revisions","date":"2021-03-03T00:00:00+00:00","index":"","fulltext":""},{"type":"editorInvitedReview","content":"","date":"2021-02-23T00:00:00+00:00","index":2,"fulltext":"Recommendation: Reviewer's comments unavailable due to the journal's policy.\n"},{"type":"reviewerAgreed","content":"","date":"2021-02-17T00:00:00+00:00","index":3,"fulltext":""},{"type":"reviewerAgreed","content":"","date":"2021-02-14T00:00:00+00:00","index":2,"fulltext":""},{"type":"reviewerAgreed","content":"","date":"2021-01-29T00:00:00+00:00","index":1,"fulltext":""},{"type":"editorInvitedReview","content":"","date":"2021-01-29T00:00:00+00:00","index":1,"fulltext":"Recommendation: Reviewer's comments unavailable due to the journal's policy.\n"},{"type":"reviewersInvited","content":"","date":"2021-01-28T00:00:00+00:00","index":"","fulltext":""},{"type":"editorAssigned","content":"","date":"2021-01-27T00:00:00+00:00","index":"","fulltext":""},{"type":"checksComplete","content":"","date":"2021-01-26T23:00:00+00:00","index":"","fulltext":""},{"type":"editorInvited","content":"","date":"2021-01-26T23:00:00+00:00","index":"","fulltext":""},{"type":"submitted","content":"","date":"2021-01-26T00:00:00+00:00","index":"","fulltext":""}],"status":"published","journal":{"display":true,"email":"[email protected]","identity":"journal-of-advanced-ceramics","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":false,"externalIdentity":"jace","sideBox":"Learn more about [Journal of Advanced Ceramics](http://link.springer.com/journal/40145)","snPcode":"","submissionUrl":"https://www.editorialmanager.com/jace/default.aspx","title":"Journal of Advanced Ceramics","twitterHandle":"","acdcEnabled":true,"dfaEnabled":false,"editorialSystem":"em","reportingPortfolio":"BMC/SO AJ","inReviewEnabled":true,"inReviewRevisionsEnabled":true}}],"origin":"","ownerIdentity":"09093019-54d5-4e6f-a74a-d93df34271c9","owner":[],"postedDate":"February 10th, 2021","published":true,"recentEditorialEvents":[],"rejectedJournal":[],"revision":"","amendment":"","status":"under-review","subjectAreas":[{"id":2355878,"name":"Ceramics"}],"tags":[],"updatedAt":"2021-04-18T14:20:48+00:00","versionOfRecord":[],"versionCreatedAt":"2021-02-10 19:38:32","video":"","vorDoi":"","vorDoiUrl":"","workflowStages":[]},"version":"v1","identity":"rs-184920","journalConfig":"researchsquare"},"__N_SSP":true},"page":"/article/[identity]/[[...version]]","query":{"redirect":"/article/rs-184920","identity":"rs-184920","version":["v1"]},"buildId":"WrCJVZZCHTDjtuVLN7oU0","isFallback":false,"isExperimentalCompile":false,"dynamicIds":[84888],"gssp":true,"scriptLoader":[]}