Preparation and characterizing of microsphere-shaped-flower-rod- like NiCo-LDHs/rGO/Bi 2 S 3 nanocomposite electrode for supercapacitor application

Preparation and characterizing of microsphere-shaped-flower-rod- like NiCo-LDHs/rGO/Bi 2 S 3 nanocomposite electrode for supercapacitor application | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Preparation and characterizing of microsphere-shaped-flower-rod- like NiCo-LDHs/rGO/Bi 2 S 3 nanocomposite electrode for supercapacitor application B. B. Sahoo, V. S. Pandey, D. N. Thatoi, Namita Dash, Manoj K. Nayak This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-7370034/v1 This work is licensed under a CC BY 4.0 License Status: Under Review Version 1 posted 9 You are reading this latest preprint version Abstract A supercapacitor (SC) is a device that possesses outstanding potential to impart significant breakthroughs in energy storage. The current study deals with an experimental investigation in developing NiCo layered double hydroxides/reduced graphene oxide/ Bismuth sulfide ( )nanocomposites and exploring its characterization as well as electrochemical measurement. Efficient straightforward and adaptable synthetic approach is implemented to prepare the nanocomposite. In the present investigation XRD, SEM, EDS, TEM, Raman spectroscopy are applied for the characterization while CV, GCD are used for electrochemical measurement of the nanocomposite. In the present study, the as-prepared nanocomposite exhibits rod type structure. The nanocomposite exhibits a decreased band gap and greater free electrons, suggesting that the nanocomposite favors electron transport. The nanocomposite possesses significantly high specific capacitance value of 1139 F/g at current density (CD) of 1 A/g compared to that of NiCo-LDHs/rGOand . Further, the nanocomposite exhibits energy density (ED) of 36.86 Wh/kg and power density (PD) of 919 W/kg at a current density of 1 A/g. Because of its non-toxicity, plentiful availability, environment friendly and cost effectiveness, the as-developed nanocomposite finds significant real-world applications in SCs. Energy storage Supercapacitor rGO Nanorods Nanocomposite Full Text Additional Declarations No competing interests reported. Cite Share Download PDF Status: Under Review Version 1 posted Editorial decision: Revision requested 30 Sep, 2025 Reviews received at journal 25 Sep, 2025 Reviews received at journal 18 Sep, 2025 Reviewers agreed at journal 17 Sep, 2025 Reviewers agreed at journal 17 Sep, 2025 Reviewers invited by journal 17 Sep, 2025 Editor assigned by journal 09 Sep, 2025 Submission checks completed at journal 06 Sep, 2025 First submitted to journal 06 Sep, 2025 You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. Our growing team is made up of researchers and industry professionals working together to solve the most critical problems facing scientific publishing. Also discoverable on Platform About Our Team In Review Editorial Policies Advisory Board Help Center Resources Author Services Accessibility API Access RSS feed Manage Cookie Preferences © Research Square 2026 | ISSN 2693-5015 (online) Privacy Policy Terms of Service Do Not Sell My Personal Information {"props":{"pageProps":{"initialData":{"identity":"rs-7370034","acceptedTermsAndConditions":true,"allowDirectSubmit":false,"archivedVersions":[],"articleType":"Research Article","associatedPublications":[],"authors":[{"id":520598317,"identity":"8c950155-1332-4959-b5ee-588cf00ef5df","order_by":0,"name":"B. B. 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