Optimization of the Photocatalytic Testing Setup Using FDM 3D Printing Technology

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Abstract

Abstract This paper presents an evaluation of the suitability of various thermoplastic materials (ASA, PC/ABS, PETG/GF) for 3D printing (Fused Deposition Modelling method) of holders designed to secure thin silicon, and other substrates, with active materials for use in photocatalytic degradation of organic compounds in aqueous solutions. To minimize the impact of the holder on the photocatalysis process, the physicochemical and mechanical properties of the printed components were analysed. The results showed that the PETG/GF filament has minimal interaction with reactive media, strong chemical and UV resistance, and desirable mechanical properties. After analysing the test results, it was decided to use these materials to produce the holder. The FDM-designed and fabricated flower-shaped holder, constructed from PETG/GF, resulted in an over 20% increase in photocatalytic process efficiency. This improvement was attributed to both the increased active surface area of the photocatalyst and the optimized geometry, which enhanced light exposure and solution mixing.
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Optimization of the Photocatalytic Testing Setup Using FDM 3D Printing Technology | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Optimization of the Photocatalytic Testing Setup Using FDM 3D Printing Technology Afrodyta Daskalakis, Patrycja Suchorska-Woźniak, Ryszard Korbutowicz, and 1 more This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-7480524/v1 This work is licensed under a CC BY 4.0 License Status: Published Journal Publication published 19 Feb, 2026 Read the published version in The International Journal of Advanced Manufacturing Technology → Version 1 posted 5 You are reading this latest preprint version Abstract This paper presents an evaluation of the suitability of various thermoplastic materials (ASA, PC/ABS, PETG/GF) for 3D printing (Fused Deposition Modelling method) of holders designed to secure thin silicon, and other substrates, with active materials for use in photocatalytic degradation of organic compounds in aqueous solutions. To minimize the impact of the holder on the photocatalysis process, the physicochemical and mechanical properties of the printed components were analysed. The results showed that the PETG/GF filament has minimal interaction with reactive media, strong chemical and UV resistance, and desirable mechanical properties. After analysing the test results, it was decided to use these materials to produce the holder. The FDM-designed and fabricated flower-shaped holder, constructed from PETG/GF, resulted in an over 20% increase in photocatalytic process efficiency. This improvement was attributed to both the increased active surface area of the photocatalyst and the optimized geometry, which enhanced light exposure and solution mixing. Additive Manufacturing Fused Deposition Modelling Thin films Ga2O3 Photocatalysis Optimization Full Text Cite Share Download PDF Status: Published Journal Publication published 19 Feb, 2026 Read the published version in The International Journal of Advanced Manufacturing Technology → Version 1 posted Editorial decision: Major Revisions Needed 01 Dec, 2025 Reviewers agreed at journal 06 Oct, 2025 Reviewers invited by journal 06 Oct, 2025 Editor assigned by journal 18 Sep, 2025 First submitted to journal 16 Sep, 2025 You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. 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