Investigation on structural, magnetic, dielectric and transport properties of xNi0.3Co0.2Zn0.5Fe2O4-(1-x)BaZr0.045Mn0.1Ti0.855O3 multiferroic composites
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Abstract Structural, magnetic, dielectric and transport features was studied thoroughly in various x Ni 0.3 Co 0.2 Zn 0.5 Fe 2 O 4 -(1- x )BaZr 0.045 Mn 0.1 Ti 0.855 O 3 . Ferromagnetic and ferroelectric phases of the mentioned composition were achieved through conventional solid state reaction method. X-ray diffraction (XRD) patterns were used in the structural study, and Fourier transform infrared ray (FTIR) was used for additional study of the structure. XRD results revealed that composites have a biphasic spinel-perovskite structure. The microstructural characteristics of the samples under study were examined using images from field emission scanning electron microscopy. Magnetoelectrically coupled composites exhibit a clear change in lattice, magnetic, and dielectric characteristics with the variation of ferrite concentration. Magnetic studies reveal that increasing ferrite content reduces magnetic loss while improving initial permeability, relative quality factor, and magnetization. M-H hysteresis loop confirmed that all studied specimens retained their usual ferromagnetic properties. With an increase in ferrite content, the dielectric constant of the studied samples decreases except for the x = 0.20 composite. The highest dielectric response was obtained for x = 0.20, which might be a potential candidate for forthcoming multifunctional devices. AC conductivity investigation showed that the conduction mechanism fitted Jonscher's power law and was ascribed to tiny polaron hopping. The Nyquist plot was used to evaluate complex impedance, ensuring that grain and grain boundary resistance prevailed. These results expand our understanding of the structural, morphological, magnetic, dielectric, and transport characteristics of the studied samples, emphasizing their potential applications in advanced electronics and energy sector.
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Investigation on structural, magnetic, dielectric and transport properties of xNi0.3Co0.2Zn0.5Fe2O4-(1-x)BaZr0.045Mn0.1Ti0.855O3 multiferroic composites | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Short Report Investigation on structural, magnetic, dielectric and transport properties of x Ni 0.3 Co 0.2 Zn 0.5 Fe 2 O 4 -(1- x )BaZr 0.045 Mn 0.1 Ti 0.855 O 3 multiferroic composites F. Alam, Bablu Chandra Das, Harinarayan Das, S. C. Mazumdar This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-7452321/v1 This work is licensed under a CC BY 4.0 License Status: Published Journal Publication published 28 Mar, 2026 Read the published version in Discover Materials → Version 1 posted 11 You are reading this latest preprint version Abstract Structural, magnetic, dielectric and transport features was studied thoroughly in various x Ni 0.3 Co 0.2 Zn 0.5 Fe 2 O 4 -(1- x )BaZr 0.045 Mn 0.1 Ti 0.855 O 3 . Ferromagnetic and ferroelectric phases of the mentioned composition were achieved through conventional solid state reaction method. X-ray diffraction (XRD) patterns were used in the structural study, and Fourier transform infrared ray (FTIR) was used for additional study of the structure. XRD results revealed that composites have a biphasic spinel-perovskite structure. The microstructural characteristics of the samples under study were examined using images from field emission scanning electron microscopy. Magnetoelectrically coupled composites exhibit a clear change in lattice, magnetic, and dielectric characteristics with the variation of ferrite concentration. Magnetic studies reveal that increasing ferrite content reduces magnetic loss while improving initial permeability, relative quality factor, and magnetization. M-H hysteresis loop confirmed that all studied specimens retained their usual ferromagnetic properties. With an increase in ferrite content, the dielectric constant of the studied samples decreases except for the x = 0.20 composite. The highest dielectric response was obtained for x = 0.20, which might be a potential candidate for forthcoming multifunctional devices. AC conductivity investigation showed that the conduction mechanism fitted Jonscher's power law and was ascribed to tiny polaron hopping. The Nyquist plot was used to evaluate complex impedance, ensuring that grain and grain boundary resistance prevailed. These results expand our understanding of the structural, morphological, magnetic, dielectric, and transport characteristics of the studied samples, emphasizing their potential applications in advanced electronics and energy sector. X-ray diffraction FTIR Microstructure Ferrites Ferroelectrics dielectric Magnetic Full Text Additional Declarations No competing interests reported. Cite Share Download PDF Status: Published Journal Publication published 28 Mar, 2026 Read the published version in Discover Materials → Version 1 posted Editorial decision: Revision requested 17 Oct, 2025 Reviews received at journal 14 Oct, 2025 Reviewers agreed at journal 06 Oct, 2025 Reviews received at journal 27 Sep, 2025 Reviewers agreed at journal 20 Sep, 2025 Reviewers agreed at journal 14 Sep, 2025 Reviewers invited by journal 14 Sep, 2025 Editor invited by journal 11 Sep, 2025 Editor assigned by journal 29 Aug, 2025 Submission checks completed at journal 29 Aug, 2025 First submitted to journal 25 Aug, 2025 You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. Our growing team is made up of researchers and industry professionals working together to solve the most critical problems facing scientific publishing. Also discoverable on Platform About Our Team In Review Editorial Policies Advisory Board Help Center Resources Author Services Accessibility API Access RSS feed Manage Cookie Preferences © Research Square 2026 | ISSN 2693-5015 (online) Privacy Policy Terms of Service Do Not Sell My Personal Information {"props":{"pageProps":{"initialData":{"identity":"rs-7452321","acceptedTermsAndConditions":true,"allowDirectSubmit":false,"archivedVersions":[],"articleType":"Short Report","associatedPublications":[],"authors":[{"id":517970330,"identity":"a0c8d451-eded-4993-9596-07d1bc8e84ca","order_by":0,"name":"F. 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\u003cem\u003ex\u003c/em\u003eNi\u003csub\u003e0.3\u003c/sub\u003eCo\u003csub\u003e0.2\u003c/sub\u003eZn\u003csub\u003e0.5\u003c/sub\u003eFe\u003csub\u003e2\u003c/sub\u003eO\u003csub\u003e4\u003c/sub\u003e-(1-\u003cem\u003ex\u003c/em\u003e)BaZr\u003csub\u003e0.045\u003c/sub\u003eMn\u003csub\u003e0.1\u003c/sub\u003eTi\u003csub\u003e0.855\u003c/sub\u003eO\u003csub\u003e3\u003c/sub\u003e. Ferromagnetic and ferroelectric phases of the mentioned composition were achieved through conventional solid state reaction method. X-ray diffraction (XRD) patterns were used in the structural study, and Fourier transform infrared ray (FTIR) was used for additional study of the structure. XRD results revealed that composites have a biphasic spinel-perovskite structure. The microstructural characteristics of the samples under study were examined using images from field emission scanning electron microscopy. Magnetoelectrically coupled composites exhibit a clear change in lattice, magnetic, and dielectric characteristics with the variation of ferrite concentration. Magnetic studies reveal that increasing ferrite content reduces magnetic loss while improving initial permeability, relative quality factor, and magnetization. M-H hysteresis loop confirmed that all studied specimens retained their usual ferromagnetic properties. With an increase in ferrite content, the dielectric constant of the studied samples decreases except for the x\u0026thinsp;=\u0026thinsp;0.20 composite. The highest dielectric response was obtained for \u003cem\u003ex\u003c/em\u003e\u0026thinsp;=\u0026thinsp;0.20, which might be a potential candidate for forthcoming multifunctional devices. AC conductivity investigation showed that the conduction mechanism fitted Jonscher's power law and was ascribed to tiny polaron hopping. The Nyquist plot was used to evaluate complex impedance, ensuring that grain and grain boundary resistance prevailed. These results expand our understanding of the structural, morphological, magnetic, dielectric, and transport characteristics of the studied samples, emphasizing their potential applications in advanced electronics and energy sector.\u003c/p\u003e","manuscriptTitle":"Investigation on structural, magnetic, dielectric and transport properties of xNi0.3Co0.2Zn0.5Fe2O4-(1-x)BaZr0.045Mn0.1Ti0.855O3 multiferroic composites","msid":"","msnumber":"","nonDraftVersions":[{"code":1,"date":"2025-09-22 14:55:57","doi":"10.21203/rs.3.rs-7452321/v1","editorialEvents":[{"type":"communityComments","content":0},{"type":"decision","content":"Revision requested","date":"2025-10-17T09:41:10+00:00","index":"","fulltext":""},{"type":"editorInvitedReview","content":"","date":"2025-10-14T22:35:17+00:00","index":"hide","fulltext":""},{"type":"reviewerAgreed","content":"278708967687578690491641872552493348471","date":"2025-10-06T21:07:11+00:00","index":"hide","fulltext":""},{"type":"editorInvitedReview","content":"","date":"2025-09-27T11:51:29+00:00","index":"hide","fulltext":""},{"type":"reviewerAgreed","content":"97772009769332087007310816282783686753","date":"2025-09-20T08:37:10+00:00","index":"hide","fulltext":""},{"type":"reviewerAgreed","content":"293934550757836873240881147437217272088","date":"2025-09-14T17:17:06+00:00","index":"hide","fulltext":""},{"type":"reviewersInvited","content":"","date":"2025-09-14T17:13:05+00:00","index":"","fulltext":""},{"type":"editorInvited","content":"","date":"2025-09-11T10:23:35+00:00","index":"","fulltext":""},{"type":"editorAssigned","content":"","date":"2025-08-29T09:41:01+00:00","index":"","fulltext":""},{"type":"checksComplete","content":"","date":"2025-08-29T09:40:47+00:00","index":"","fulltext":""},{"type":"submitted","content":"Discover Materials","date":"2025-08-25T09:41:38+00:00","index":"","fulltext":""}],"status":"published","journal":{"display":true,"email":"[email protected]","identity":"discover-materials","isNatureJournal":false,"hasQc":true,"allowDirectSubmit":false,"externalIdentity":"dime","sideBox":"Learn more about [Discover Materials](https://www.springer.com/journal/43939)","snPcode":"","submissionUrl":"","title":"Discover Materials","twitterHandle":"","acdcEnabled":true,"dfaEnabled":true,"editorialSystem":"stoa","reportingPortfolio":"Discover Series","inReviewEnabled":true,"inReviewRevisionsEnabled":true}}],"origin":"","ownerIdentity":"61639477-a0d1-4ee2-b47a-48c0e342a328","owner":[],"postedDate":"September 22nd, 2025","published":true,"recentEditorialEvents":[],"rejectedJournal":[],"revision":"","amendment":"","status":"published-in-journal","subjectAreas":[],"tags":[],"updatedAt":"2026-03-30T16:21:01+00:00","versionOfRecord":{"articleIdentity":"rs-7452321","link":"https://doi.org/10.1007/s43939-026-00621-7","journal":{"identity":"discover-materials","isVorOnly":false,"title":"Discover Materials"},"publishedOn":"2026-03-28 16:10:05","publishedOnDateReadable":"March 28th, 2026"},"versionCreatedAt":"2025-09-22 14:55:57","video":"","vorDoi":"10.1007/s43939-026-00621-7","vorDoiUrl":"https://doi.org/10.1007/s43939-026-00621-7","workflowStages":[]},"version":"v1","identity":"rs-7452321","journalConfig":"researchsquare"},"__N_SSP":true},"page":"/article/[identity]/[[...version]]","query":{"redirect":"/article/rs-7452321","identity":"rs-7452321","version":["v1"]},"buildId":"8U1c8b4HqxoKbykW_rLl7","isFallback":false,"isExperimentalCompile":false,"dynamicIds":[84888],"gssp":true,"scriptLoader":[]}
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