Gelcast Zirconia Ceramics With High Strength and Simultaneously High Translucency for Dental Applications

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Developed gelcasting 3Y-TZP ceramics achieved high biaxial strength (1184 MPa) and translucency (46.7% at 600 nm) for dental restorations, overcoming the strength-translucency trade-off.

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The paper investigated how to fabricate machinable 3 mol% yttria-stabilized tetragonal zirconia (3Y-TZP) ceramics with both high strength and enhanced translucency using a gelcasting processing route based on fine mesostructured zirconia particles, then characterized shrinkage, density, microstructure, surface roughness, hardness, biaxial strength, and total forward transmittance. Sintered samples achieved an average biaxial strength of 1184 MPa and 46.7% total forward transmittance at 600 nm for a 0.5 mm thick specimen, with homogeneous structure, grain sizes up to 620 nm, and a purely tetragonal phase composition. A stated caveat is that the work is a Research Square preprint and not peer reviewed in a journal. This paper does not explicitly discuss endometriosis or adenomyosis; it was included in the corpus via a keyword match in the upstream search index.

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Abstract

Abstract Translucent zirconia represents a favourite material for monolithic ceramic dental restorations. However, materials approaches employed so far to improve the translucency of zirconia ceramics are accompanied by a significant decline in strength. Thus, we aimed to develop dental 3Y-TZP ceramics that can provide excellent strength and, simultaneously, enhanced translucency. In this investigation, machinable tetragonal zirconia ceramics based on fine mesostructured zirconia particles stabilized with 3 mol% of yttria and prepared by the gelcasting processing method were developed. Properties of sintered samples were characterised, namely: shrinkage, density, structure, surface roughness, hardness, biaxial strength, and total forward transmittance. Zirconia ceramics with an average biaxial strength of 1184 MPa and a total forward transmittance of 46.7% for a 0.5 mm thick sample at a wavelength of 600 nm were obtained. These ceramics exhibited homogeneous structure with grains sizes up to 620 nm and purely tetragonal phase composition. The developed ceramics provided a favourable combination of high translucency comparable even with the mixed cubic/tetragonal structure of a common 4Y-TZP, and very high strength that is achievable only in the pure tetragonal 3Y-TZP.
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Gelcast Zirconia Ceramics With High Strength and Simultaneously High Translucency for Dental Applications | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Research Article Gelcast Zirconia Ceramics With High Strength and Simultaneously High Translucency for Dental Applications Jaroslav Kastyl, Zdenek Chlup, Vaclav Pouchly, Lu Song, Erik Scasnovic, and 1 more This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-736845/v1 This work is licensed under a CC BY 4.0 License Status: Posted Version 1 posted You are reading this latest preprint version Abstract Translucent zirconia represents a favourite material for monolithic ceramic dental restorations. However, materials approaches employed so far to improve the translucency of zirconia ceramics are accompanied by a significant decline in strength. Thus, we aimed to develop dental 3Y-TZP ceramics that can provide excellent strength and, simultaneously, enhanced translucency. In this investigation, machinable tetragonal zirconia ceramics based on fine mesostructured zirconia particles stabilized with 3 mol% of yttria and prepared by the gelcasting processing method were developed. Properties of sintered samples were characterised, namely: shrinkage, density, structure, surface roughness, hardness, biaxial strength, and total forward transmittance. Zirconia ceramics with an average biaxial strength of 1184 MPa and a total forward transmittance of 46.7% for a 0.5 mm thick sample at a wavelength of 600 nm were obtained. These ceramics exhibited homogeneous structure with grains sizes up to 620 nm and purely tetragonal phase composition. The developed ceramics provided a favourable combination of high translucency comparable even with the mixed cubic/tetragonal structure of a common 4Y-TZP, and very high strength that is achievable only in the pure tetragonal 3Y-TZP. Ceramics zirconia nanoparticles gelcasting biaxial strength translucency dental restoration Full Text Supplementary Files Electronicsupplementarymaterial.docx Electronic supplementary material Cite Share Download PDF Status: Posted Version 1 posted You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. Our growing team is made up of researchers and industry professionals working together to solve the most critical problems facing scientific publishing. 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