Synthesis and characterization of Modified Bismuth ferrite (1-x)BiFeO 3 - x(BiK)Ti/MnO 3 , (x=0.15, 0.20)

Synthesis and characterization of Modified Bismuth ferrite (1-x)BiFeO 3 - x(BiK)Ti/MnO 3 , (x=0.15, 0.20) | Research Square window.SnipcartSettings = { analytics: { enabled: false } }; (function() { var accessVector = localStorage.getItem('access_vector') || ''; window.dataLayer = window.dataLayer || []; if (accessVector) { window.dataLayer.push({ user: { profile: { profileInfo: { snid: accessVector } } } }); } })(); (function(w,d,s,l,i){w[l]=w[l]||[];w[l].push({'gtm.start':new Date().getTime(),event:'gtm.js'});var f=d.getElementsByTagName(s)[0],j=d.createElement(s),dl=l!='dataLayer'?'&l='+l:'';j.async=true;j.src='https://www.googletagmanager.com/gtm.js?id='+i+dl;f.parentNode.insertBefore(j,f);})(window,document,'script','dataLayer','GTM-K279D39R'); Browse Preprints In Review Journals COVID-19 Preprints AJE Video Bytes Research Tools Research Promotion AJE Professional Editing AJE Rubriq About Preprint Platform In Review Editorial Policies Our Team Advisory Board Help Center Sign In Submit a Preprint Cite Share Download PDF Short Report Synthesis and characterization of Modified Bismuth ferrite (1-x)BiFeO 3 - x(BiK)Ti/MnO 3 , (x=0.15, 0.20) S. K. Sourav, R. N. P. Choudhary, Umakant Prasad This is a preprint; it has not been peer reviewed by a journal. https://doi.org/ 10.21203/rs.3.rs-4509058/v1 This work is licensed under a CC BY 4.0 License Status: Published Journal Publication published 14 Mar, 2025 Read the published version in Journal of Electroceramics → Version 1 posted 13 You are reading this latest preprint version Abstract In present era main aim of the researchers is to develop lead free material for ferroelectric material device. Ceramics of perovskite compounds were successfully synthesized using a chemical decomposition method, with the composition (1-x) BiFeO 3 -x(Bi K)TiMnO 3 , where x was varied at 0.15 and 0.20. The confirmation of compound creation was based on the analysis of Crystelloplotic XRD pattern data. The BKTM 15% exhibits an average grain size of 0.41 µm, while BKTM 20% shows 0.40 µm. Energy-dispersive X-ray analysis detected elements such as Bi, Fe, Na, K, Ti, and Mn. Modulus property exploration revealed non-Debye model relaxation behavior, observed particularly for sensor technology applications. To investigate the relaxation and conduction mechanisms in these samples were conducted at different temperatures and recurrence. Additionally, the scanning electron microscope (SEM) was employed to examine particle allocation and the location of grain boundaries. Impedance spectroscopic studies covered a wide temperature range (300-780K) and a broad recurrence range (10 3 -10 6 Hz). Complex plane and Impedance scale are semicircular arcs, which related to semiconducting character of the sample. Modulus and Ac conductivity rhombohedral Impedance scale plot Scanning electron microscope (SEM) Complex plane plots Full Text Additional Declarations No competing interests reported. Cite Share Download PDF Status: Published Journal Publication published 14 Mar, 2025 Read the published version in Journal of Electroceramics → Version 1 posted Editorial decision: Revision requested 22 Sep, 2024 Reviews received at journal 27 Jul, 2024 Reviewers agreed at journal 23 Jul, 2024 Reviewers agreed at journal 22 Jul, 2024 Reviewers agreed at journal 21 Jul, 2024 Reviewers agreed at journal 21 Jul, 2024 Reviews received at journal 01 Jul, 2024 Reviewers agreed at journal 23 Jun, 2024 Reviewers agreed at journal 22 Jun, 2024 Reviewers invited by journal 22 Jun, 2024 Submission checks completed at journal 03 Jun, 2024 Editor assigned by journal 03 Jun, 2024 First submitted to journal 31 May, 2024 You are reading this latest preprint version Research Square lets you share your work early, gain feedback from the community, and start making changes to your manuscript prior to peer review in a journal. As a division of Research Square Company, we’re committed to making research communication faster, fairer, and more useful. We do this by developing innovative software and high quality services for the global research community. Our growing team is made up of researchers and industry professionals working together to solve the most critical problems facing scientific publishing. Also discoverable on Platform About Our Team In Review Editorial Policies Advisory Board Help Center Resources Author Services Accessibility API Access RSS feed Manage Cookie Preferences © Research Square 2026 | ISSN 2693-5015 (online) Privacy Policy Terms of Service Do Not Sell My Personal Information {"props":{"pageProps":{"initialData":{"identity":"rs-4509058","acceptedTermsAndConditions":true,"allowDirectSubmit":false,"archivedVersions":[],"articleType":"Short Report","associatedPublications":[],"authors":[{"id":313038602,"identity":"9d49c7ff-bef0-45b6-9298-b8640d23dbcb","order_by":0,"name":"S. K. 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Ceramics of perovskite compounds were successfully synthesized using a chemical decomposition method, with the composition (1-x) BiFeO\u003csub\u003e3\u003c/sub\u003e-x(Bi K)TiMnO\u003csub\u003e3\u003c/sub\u003e, where x was varied at 0.15 and 0.20. The confirmation of compound creation was based on the analysis of Crystelloplotic XRD pattern data. The BKTM 15% exhibits an average grain size of 0.41 \u0026micro;m, while BKTM 20% shows 0.40 \u0026micro;m. Energy-dispersive X-ray analysis detected elements such as Bi, Fe, Na, K, Ti, and Mn. Modulus property exploration revealed non-Debye model relaxation behavior, observed particularly for sensor technology applications. To investigate the relaxation and conduction mechanisms in these samples were conducted at different temperatures and recurrence. Additionally, the scanning electron microscope (SEM) was employed to examine particle allocation and the location of grain boundaries. 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