Novel Hydrothermal Synthesis of Pure and Doped Ammonium and Potassium Titanyl Phosphates using a Green Heterogeneous Reaction

Vital inroganic materials are often inefficienty prepared in terms of time, reagents, and manpower. Hydrothermal methods in particular often take many days or even weeks to prepare the desired materials. In this communication, we demonstrate a novel heterogeneous, green synthesis route and the crystal lattice parameters of several pure and intermediate ammonium and potassium titanyl phosphates, representing a significant improvement over existing syntheses in reaction time and precursors used.